Synthesis and characterization of iron(ii)-curcumin complex / Siti Nor Aini Md Shari

Curcumin is a yellow powder solid which is widely used in medical area.However this study focusing on photonic area. The preparation of Fe(II)-curcumin complex by different ratio (1:1, 1:1.5 and 1:2) and temperature at 25oC and 40oC was studied. Only Curcumin vary in mole ratio not the metal Iron(II...

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Main Author: Md Shari, Siti Nor Aini
Format: Thesis
Language:English
Published: 2010
Online Access:https://ir.uitm.edu.my/id/eprint/100024/2/100024.pdf
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spelling my-uitm-ir.1000242024-08-21T23:33:13Z Synthesis and characterization of iron(ii)-curcumin complex / Siti Nor Aini Md Shari 2010 Md Shari, Siti Nor Aini Curcumin is a yellow powder solid which is widely used in medical area.However this study focusing on photonic area. The preparation of Fe(II)-curcumin complex by different ratio (1:1, 1:1.5 and 1:2) and temperature at 25oC and 40oC was studied. Only Curcumin vary in mole ratio not the metal Iron(II). After that, the samples were characterized by using UV-Vis spectroscopy, Fluorescence spectroscopy, FTIR and TGA. For overall in UV-Vis analysis the absorbance is increased when temperature increase. λmax also increased and the blue and red shift observed. Meanwhile for fluorescence result, 1:2 at 40oC is the optimum Stoke’s shift. In FTIR analysis, the changes in shift occurs indicate complexation involved. In TGA analysis, the all complex undergoes decomposition until formed iron oxide. As a conclusion, The optimum result is 1:2 at 40oC. 2010 Thesis https://ir.uitm.edu.my/id/eprint/100024/ https://ir.uitm.edu.my/id/eprint/100024/2/100024.pdf text en public degree Universiti Teknologi MARA (UiTM) Faculty of Applied Science
institution Universiti Teknologi MARA
collection UiTM Institutional Repository
language English
description Curcumin is a yellow powder solid which is widely used in medical area.However this study focusing on photonic area. The preparation of Fe(II)-curcumin complex by different ratio (1:1, 1:1.5 and 1:2) and temperature at 25oC and 40oC was studied. Only Curcumin vary in mole ratio not the metal Iron(II). After that, the samples were characterized by using UV-Vis spectroscopy, Fluorescence spectroscopy, FTIR and TGA. For overall in UV-Vis analysis the absorbance is increased when temperature increase. λmax also increased and the blue and red shift observed. Meanwhile for fluorescence result, 1:2 at 40oC is the optimum Stoke’s shift. In FTIR analysis, the changes in shift occurs indicate complexation involved. In TGA analysis, the all complex undergoes decomposition until formed iron oxide. As a conclusion, The optimum result is 1:2 at 40oC.
format Thesis
qualification_level Bachelor degree
author Md Shari, Siti Nor Aini
spellingShingle Md Shari, Siti Nor Aini
Synthesis and characterization of iron(ii)-curcumin complex / Siti Nor Aini Md Shari
author_facet Md Shari, Siti Nor Aini
author_sort Md Shari, Siti Nor Aini
title Synthesis and characterization of iron(ii)-curcumin complex / Siti Nor Aini Md Shari
title_short Synthesis and characterization of iron(ii)-curcumin complex / Siti Nor Aini Md Shari
title_full Synthesis and characterization of iron(ii)-curcumin complex / Siti Nor Aini Md Shari
title_fullStr Synthesis and characterization of iron(ii)-curcumin complex / Siti Nor Aini Md Shari
title_full_unstemmed Synthesis and characterization of iron(ii)-curcumin complex / Siti Nor Aini Md Shari
title_sort synthesis and characterization of iron(ii)-curcumin complex / siti nor aini md shari
granting_institution Universiti Teknologi MARA (UiTM)
granting_department Faculty of Applied Science
publishDate 2010
url https://ir.uitm.edu.my/id/eprint/100024/2/100024.pdf
_version_ 1811769047263477760