Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali

Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali

This research aims at investigating Heck reaction in ionic liquid accelerated by microwave irradiation. Five different conditions have been utilized in order to accomplish this research study. Three of the conditions utililized Heck reaction in ionic liquids and other two conditions utilized heck re...

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Main Author: Mohd Sali, Siti Zarina
Format: Thesis
Language:English
Published: 2008
Subjects:
Pharmaceutical chemistry
Online Access:https://ir.uitm.edu.my/id/eprint/101884/1/101884.PDF
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spelling my-uitm-ir.1018842024-09-28T23:35:03Z Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali 2008 Mohd Sali, Siti Zarina Pharmaceutical chemistry This research aims at investigating Heck reaction in ionic liquid accelerated by microwave irradiation. Five different conditions have been utilized in order to accomplish this research study. Three of the conditions utililized Heck reaction in ionic liquids and other two conditions utilized heck reaction in ionic liquids accelerated by microwave irradiation. When Heck reaction in ionic liquids, the desired stilbene able to produced with the yield 26.3% (with 4-iodoanisole as starting materials for 12 hours) and 33.85% (with 4-Iodophenylbenzyl ether as starting materials for I 2 hours) and 7.98% (with 4-iodoanisole as starting materials leave for 21 hour). While when Heck reaction accelerated by microwave irradiation, the desired stilbene able to produced with the yield 61.35% ( with the ionic liquids) and 68.27% (with DMF). Preparative TLC were used to confirm the desired product. 2008 Thesis https://ir.uitm.edu.my/id/eprint/101884/ https://ir.uitm.edu.my/id/eprint/101884/1/101884.PDF text en public degree Universiti Teknologi MARA (Kampus Puncak Alam) Faculty of Pharmacy Feroz, Fareeda
institution Universiti Teknologi MARA
collection UiTM Institutional Repository
language English
advisor Feroz, Fareeda
topic Pharmaceutical chemistry
spellingShingle Pharmaceutical chemistry
Mohd Sali, Siti Zarina
Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali
description This research aims at investigating Heck reaction in ionic liquid accelerated by microwave irradiation. Five different conditions have been utilized in order to accomplish this research study. Three of the conditions utililized Heck reaction in ionic liquids and other two conditions utilized heck reaction in ionic liquids accelerated by microwave irradiation. When Heck reaction in ionic liquids, the desired stilbene able to produced with the yield 26.3% (with 4-iodoanisole as starting materials for 12 hours) and 33.85% (with 4-Iodophenylbenzyl ether as starting materials for I 2 hours) and 7.98% (with 4-iodoanisole as starting materials leave for 21 hour). While when Heck reaction accelerated by microwave irradiation, the desired stilbene able to produced with the yield 61.35% ( with the ionic liquids) and 68.27% (with DMF). Preparative TLC were used to confirm the desired product.
format Thesis
qualification_level Bachelor degree
author Mohd Sali, Siti Zarina
author_facet Mohd Sali, Siti Zarina
author_sort Mohd Sali, Siti Zarina
title Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali
title_short Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali
title_full Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali
title_fullStr Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali
title_full_unstemmed Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali
title_sort heck reaction in ionic liquid accelerated by microwave irradiation / siti zarina mohd sali
granting_institution Universiti Teknologi MARA (Kampus Puncak Alam)
granting_department Faculty of Pharmacy
publishDate 2008
url https://ir.uitm.edu.my/id/eprint/101884/1/101884.PDF
_version_ 1811769195297243136

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