Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali
This research aims at investigating Heck reaction in ionic liquid accelerated by microwave irradiation. Five different conditions have been utilized in order to accomplish this research study. Three of the conditions utililized Heck reaction in ionic liquids and other two conditions utilized heck re...
Saved in:
| 主要作者: | |
|---|---|
| 格式: | Thesis |
| 语言: | English |
| 出版: |
2008
|
| 主题: | |
| 在线阅读: | https://ir.uitm.edu.my/id/eprint/101884/1/101884.PDF |
| 标签: |
添加标签
没有标签, 成为第一个标记此记录!
|
| id |
my-uitm-ir.101884 |
|---|---|
| record_format |
uketd_dc |
| spelling |
my-uitm-ir.1018842024-09-28T23:35:03Z Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali 2008 Mohd Sali, Siti Zarina Pharmaceutical chemistry This research aims at investigating Heck reaction in ionic liquid accelerated by microwave irradiation. Five different conditions have been utilized in order to accomplish this research study. Three of the conditions utililized Heck reaction in ionic liquids and other two conditions utilized heck reaction in ionic liquids accelerated by microwave irradiation. When Heck reaction in ionic liquids, the desired stilbene able to produced with the yield 26.3% (with 4-iodoanisole as starting materials for 12 hours) and 33.85% (with 4-Iodophenylbenzyl ether as starting materials for I 2 hours) and 7.98% (with 4-iodoanisole as starting materials leave for 21 hour). While when Heck reaction accelerated by microwave irradiation, the desired stilbene able to produced with the yield 61.35% ( with the ionic liquids) and 68.27% (with DMF). Preparative TLC were used to confirm the desired product. 2008 Thesis https://ir.uitm.edu.my/id/eprint/101884/ https://ir.uitm.edu.my/id/eprint/101884/1/101884.PDF text en public degree Universiti Teknologi MARA (Kampus Puncak Alam) Faculty of Pharmacy Feroz, Fareeda |
| institution |
Universiti Teknologi MARA |
| collection |
UiTM Institutional Repository |
| language |
English |
| advisor |
Feroz, Fareeda |
| topic |
Pharmaceutical chemistry |
| spellingShingle |
Pharmaceutical chemistry Mohd Sali, Siti Zarina Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali |
| description |
This research aims at investigating Heck reaction in ionic liquid accelerated by microwave irradiation. Five different conditions have been utilized in order to accomplish this research study. Three of the conditions utililized Heck reaction in ionic liquids and other two conditions utilized heck reaction in ionic liquids accelerated by microwave irradiation. When Heck reaction in ionic liquids, the desired stilbene able to produced with the yield 26.3% (with 4-iodoanisole as starting materials for 12 hours) and 33.85% (with 4-Iodophenylbenzyl ether as starting materials for I 2 hours) and 7.98% (with 4-iodoanisole as starting materials leave for 21 hour). While when Heck reaction accelerated by microwave irradiation, the desired stilbene able to produced with the yield 61.35% ( with the ionic liquids) and 68.27% (with DMF). Preparative TLC were used to confirm the desired product. |
| format |
Thesis |
| qualification_level |
Bachelor degree |
| author |
Mohd Sali, Siti Zarina |
| author_facet |
Mohd Sali, Siti Zarina |
| author_sort |
Mohd Sali, Siti Zarina |
| title |
Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali |
| title_short |
Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali |
| title_full |
Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali |
| title_fullStr |
Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali |
| title_full_unstemmed |
Heck reaction in ionic liquid accelerated by microwave irradiation / Siti Zarina Mohd Sali |
| title_sort |
heck reaction in ionic liquid accelerated by microwave irradiation / siti zarina mohd sali |
| granting_institution |
Universiti Teknologi MARA (Kampus Puncak Alam) |
| granting_department |
Faculty of Pharmacy |
| publishDate |
2008 |
| url |
https://ir.uitm.edu.my/id/eprint/101884/1/101884.PDF |
| _version_ |
1811769195297243136 |