Utilisation of nano materials in enhancing strength and durability properties of ultra high performance concrete (UHPC) / Muhd Norhasri Muhd Sidek

Hydration gel (C-S-H) is major component in binding of concrete and refining of the C-S-H gel is difficult to be done by using micro based materials. For this research, inclusion of nano materials in UHPC is expected to overcome the problem by providing ultra filler effect. In this study, the utilis...

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Main Author:	Muhd Sidek, Muhd Norhasri
Format:	Thesis
Language:	English
Published:	2016
Online Access:	https://ir.uitm.edu.my/id/eprint/18578/1/TP_MUHD%20NORHASRI%20MUHD%20SIDEK%20EC%2016_5.pdf
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spelling	my-uitm-ir.185782018-01-05T06:38:34Z Utilisation of nano materials in enhancing strength and durability properties of ultra high performance concrete (UHPC) / Muhd Norhasri Muhd Sidek 2016 Muhd Sidek, Muhd Norhasri Hydration gel (C-S-H) is major component in binding of concrete and refining of the C-S-H gel is difficult to be done by using micro based materials. For this research, inclusion of nano materials in UHPC is expected to overcome the problem by providing ultra filler effect. In this study, the utilisation of nano material in UHPC was done by using additive or replacement method for cement and UHPC mix and generated based on a series of trial modified mixes originally formulated by previous researchers. For this research, two types of nano materials were selected. Firstly, nano kaolin samples were prepared from kaolin using milling and then underwent calcination process to produce nano metakaolin. Secondly, nano clay was provided by Sigma (M) and underwent calcination process to convert to nano metaclay. Characterisation of cementitious materials were confirmed by its particle size, chemical composition and morphology properties and evaluated using Laser particle Analyser, X-Ray Fluorescence (XRF), X-Ray Diffraction (XRD) and Scanning Electron Microscope (SEM). UHPC mixes were developed by incorporating nano materials with (addition) and without (replacement) addition of metakaolin. The inclusion of nano materials as an additive and cement replacement material (without metakaolin) based on percentage of increment from 1, 3, 5, 7 and 9 %. For additive approach, addition of metakaolin was fixed to 10%. The utilisation of nano materials was assessed in terms of its cementitious, microstructures and chemical phases, strength and durability properties. In cementitious properties, cement paste were determined in terms of setting time and compressive strength. In fresh state, workability of UHPC was determined by using slump test. For strength properties compressive and flexural strength were tested. Finally, durability properties were assessed based on porosity and water absorption characteristics. UHPC specimens, containing nano materials were assessed its chemical phases and microstructure using XRD and SEM examination. Moreover, data from strength and durability properties was optimise by using Design Expert Software and mathematical equation generated. It was found that, particles of nano materials performed different morphology as compared to the OPC, kaolin and metakaolin. For cement paste, inclusion of nano materials as addition or replacement increase the water demand but also increase compressive strength as compared to the OPC and metakaolin pastes. Strength and durability properties of nano materials enhances the UHPC performance by refining microstructure, promoting pozzolanic reaction and creating nucleation process and proves from the result provided by XRD pattern and SEM micrograph analysis. 2016 Thesis https://ir.uitm.edu.my/id/eprint/18578/ https://ir.uitm.edu.my/id/eprint/18578/1/TP_MUHD%20NORHASRI%20MUHD%20SIDEK%20EC%2016_5.pdf text en public phd doctoral Universiti Teknologi MARA Faculty of Civil Engineering
institution	Universiti Teknologi MARA
collection	UiTM Institutional Repository
language	English
description	Hydration gel (C-S-H) is major component in binding of concrete and refining of the C-S-H gel is difficult to be done by using micro based materials. For this research, inclusion of nano materials in UHPC is expected to overcome the problem by providing ultra filler effect. In this study, the utilisation of nano material in UHPC was done by using additive or replacement method for cement and UHPC mix and generated based on a series of trial modified mixes originally formulated by previous researchers. For this research, two types of nano materials were selected. Firstly, nano kaolin samples were prepared from kaolin using milling and then underwent calcination process to produce nano metakaolin. Secondly, nano clay was provided by Sigma (M) and underwent calcination process to convert to nano metaclay. Characterisation of cementitious materials were confirmed by its particle size, chemical composition and morphology properties and evaluated using Laser particle Analyser, X-Ray Fluorescence (XRF), X-Ray Diffraction (XRD) and Scanning Electron Microscope (SEM). UHPC mixes were developed by incorporating nano materials with (addition) and without (replacement) addition of metakaolin. The inclusion of nano materials as an additive and cement replacement material (without metakaolin) based on percentage of increment from 1, 3, 5, 7 and 9 %. For additive approach, addition of metakaolin was fixed to 10%. The utilisation of nano materials was assessed in terms of its cementitious, microstructures and chemical phases, strength and durability properties. In cementitious properties, cement paste were determined in terms of setting time and compressive strength. In fresh state, workability of UHPC was determined by using slump test. For strength properties compressive and flexural strength were tested. Finally, durability properties were assessed based on porosity and water absorption characteristics. UHPC specimens, containing nano materials were assessed its chemical phases and microstructure using XRD and SEM examination. Moreover, data from strength and durability properties was optimise by using Design Expert Software and mathematical equation generated. It was found that, particles of nano materials performed different morphology as compared to the OPC, kaolin and metakaolin. For cement paste, inclusion of nano materials as addition or replacement increase the water demand but also increase compressive strength as compared to the OPC and metakaolin pastes. Strength and durability properties of nano materials enhances the UHPC performance by refining microstructure, promoting pozzolanic reaction and creating nucleation process and proves from the result provided by XRD pattern and SEM micrograph analysis.
format	Thesis
qualification_name	Doctor of Philosophy (PhD.)
qualification_level	Doctorate
author	Muhd Sidek, Muhd Norhasri
spellingShingle	Muhd Sidek, Muhd Norhasri Utilisation of nano materials in enhancing strength and durability properties of ultra high performance concrete (UHPC) / Muhd Norhasri Muhd Sidek
author_facet	Muhd Sidek, Muhd Norhasri
author_sort	Muhd Sidek, Muhd Norhasri
title	Utilisation of nano materials in enhancing strength and durability properties of ultra high performance concrete (UHPC) / Muhd Norhasri Muhd Sidek
title_short	Utilisation of nano materials in enhancing strength and durability properties of ultra high performance concrete (UHPC) / Muhd Norhasri Muhd Sidek
title_full	Utilisation of nano materials in enhancing strength and durability properties of ultra high performance concrete (UHPC) / Muhd Norhasri Muhd Sidek
title_fullStr	Utilisation of nano materials in enhancing strength and durability properties of ultra high performance concrete (UHPC) / Muhd Norhasri Muhd Sidek
title_full_unstemmed	Utilisation of nano materials in enhancing strength and durability properties of ultra high performance concrete (UHPC) / Muhd Norhasri Muhd Sidek
title_sort	utilisation of nano materials in enhancing strength and durability properties of ultra high performance concrete (uhpc) / muhd norhasri muhd sidek
granting_institution	Universiti Teknologi MARA
granting_department	Faculty of Civil Engineering
publishDate	2016
url	https://ir.uitm.edu.my/id/eprint/18578/1/TP_MUHD%20NORHASRI%20MUHD%20SIDEK%20EC%2016_5.pdf
_version_	1783733696001474560

Utilisation of nano materials in enhancing strength and durability properties of ultra high performance concrete (UHPC) / Muhd Norhasri Muhd Sidek

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