Effect of various loading of treated clam shells (tCS-CaCO3) filled acrylonitrile butadiene rubber (NBR) composite on cure characteristics, physical and mechanical properties / Nur Aliyyah Yunus

Clam Shells treated silane coupling agent reinforced nitrile butadiene rubber composites were successfully prepared by incorporation of different loadings of clam shells on its cure characteristics, physical and mechanical properties. Meanwhile, clam shell (CS) and calcium carbonates (CaCO3) were ch...

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Main Author: Yunus, Nur Aliyyah
Format: Thesis
Language:English
Published: 2020
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Online Access:https://ir.uitm.edu.my/id/eprint/34250/1/34250.pdf
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spelling my-uitm-ir.342502020-09-14T09:39:35Z Effect of various loading of treated clam shells (tCS-CaCO3) filled acrylonitrile butadiene rubber (NBR) composite on cure characteristics, physical and mechanical properties / Nur Aliyyah Yunus 2020-09-02 Yunus, Nur Aliyyah Polymers. Macromolecules Clam Shells treated silane coupling agent reinforced nitrile butadiene rubber composites were successfully prepared by incorporation of different loadings of clam shells on its cure characteristics, physical and mechanical properties. Meanwhile, clam shell (CS) and calcium carbonates (CaCO3) were characterized by using the fourier transform infrared (FTIR). From this FTIR result, it was showed that there was same functional group between the CS and CaCO3. The curing characteristics of the composites on optimum cure time (Tc90) were determined which the higher filler loading of tCS-CaCO3 resulted in higher cure time and it were vulcanized at 1500C using hot press. Furthermore, the mechanical properties of the NBR composites such as tensile strength had optimum value 4.736 MPa, while for the elongation at break the optimum value was 614.747 %. Both mechanical properties was increased by increasing the amount of filler loading. Other than that, for the hardness, swelling percentage (%), crosslink concentration (g/mol) and density (g/cm3) were studied which gave value of 51.4, 3.64%, 1.68 (g/mol) and 1.28 g/cm3. The good dispersion of clam shells and nitrile rubber were enhanced by treated of silane coupling agent (Si-69) that had been added in rubber composites. The presence of coupling agent also gave good curing time as well as enhanced the mechanical and physical properties of NBR composites. 2020-09 Thesis https://ir.uitm.edu.my/id/eprint/34250/ https://ir.uitm.edu.my/id/eprint/34250/1/34250.pdf text en public degree Universiti Teknologi Mara Perlis Faculty of Applied Sciences
institution Universiti Teknologi MARA
collection UiTM Institutional Repository
language English
topic Polymers
Macromolecules
spellingShingle Polymers
Macromolecules
Yunus, Nur Aliyyah
Effect of various loading of treated clam shells (tCS-CaCO3) filled acrylonitrile butadiene rubber (NBR) composite on cure characteristics, physical and mechanical properties / Nur Aliyyah Yunus
description Clam Shells treated silane coupling agent reinforced nitrile butadiene rubber composites were successfully prepared by incorporation of different loadings of clam shells on its cure characteristics, physical and mechanical properties. Meanwhile, clam shell (CS) and calcium carbonates (CaCO3) were characterized by using the fourier transform infrared (FTIR). From this FTIR result, it was showed that there was same functional group between the CS and CaCO3. The curing characteristics of the composites on optimum cure time (Tc90) were determined which the higher filler loading of tCS-CaCO3 resulted in higher cure time and it were vulcanized at 1500C using hot press. Furthermore, the mechanical properties of the NBR composites such as tensile strength had optimum value 4.736 MPa, while for the elongation at break the optimum value was 614.747 %. Both mechanical properties was increased by increasing the amount of filler loading. Other than that, for the hardness, swelling percentage (%), crosslink concentration (g/mol) and density (g/cm3) were studied which gave value of 51.4, 3.64%, 1.68 (g/mol) and 1.28 g/cm3. The good dispersion of clam shells and nitrile rubber were enhanced by treated of silane coupling agent (Si-69) that had been added in rubber composites. The presence of coupling agent also gave good curing time as well as enhanced the mechanical and physical properties of NBR composites.
format Thesis
qualification_level Bachelor degree
author Yunus, Nur Aliyyah
author_facet Yunus, Nur Aliyyah
author_sort Yunus, Nur Aliyyah
title Effect of various loading of treated clam shells (tCS-CaCO3) filled acrylonitrile butadiene rubber (NBR) composite on cure characteristics, physical and mechanical properties / Nur Aliyyah Yunus
title_short Effect of various loading of treated clam shells (tCS-CaCO3) filled acrylonitrile butadiene rubber (NBR) composite on cure characteristics, physical and mechanical properties / Nur Aliyyah Yunus
title_full Effect of various loading of treated clam shells (tCS-CaCO3) filled acrylonitrile butadiene rubber (NBR) composite on cure characteristics, physical and mechanical properties / Nur Aliyyah Yunus
title_fullStr Effect of various loading of treated clam shells (tCS-CaCO3) filled acrylonitrile butadiene rubber (NBR) composite on cure characteristics, physical and mechanical properties / Nur Aliyyah Yunus
title_full_unstemmed Effect of various loading of treated clam shells (tCS-CaCO3) filled acrylonitrile butadiene rubber (NBR) composite on cure characteristics, physical and mechanical properties / Nur Aliyyah Yunus
title_sort effect of various loading of treated clam shells (tcs-caco3) filled acrylonitrile butadiene rubber (nbr) composite on cure characteristics, physical and mechanical properties / nur aliyyah yunus
granting_institution Universiti Teknologi Mara Perlis
granting_department Faculty of Applied Sciences
publishDate 2020
url https://ir.uitm.edu.my/id/eprint/34250/1/34250.pdf
_version_ 1783734259483148288