The effect of various titanium dioxide [TiO2] loading on polymorphism of stretched polyvinylidene flouride [PVDF] /TiO2 thin film / Zulkhairul Akmal Abdul Basir

The composite of Polyvinylidene Fluoride/ Titanium dioxide (PVDF/TiO2) thin film were prepared with various loading of TiO2 using solvent casting method. The solution was stirred for 48 hours using magnetic stirrer at 600rpm. The mixture was casted into glass petri dish before being dried in the ove...

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Main Author:	Abdul Basir, Zulkhairul Akmal
Format:	Thesis
Language:	English
Published:	2020
Subjects:	Inorganic polymers Physical and theoretical chemistry Polyvinyl chloride
Online Access:	https://ir.uitm.edu.my/id/eprint/34665/1/34665.pdf
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id	my-uitm-ir.34665
record_format	uketd_dc
spelling	my-uitm-ir.346652020-09-29T05:02:05Z The effect of various titanium dioxide [TiO2] loading on polymorphism of stretched polyvinylidene flouride [PVDF] /TiO2 thin film / Zulkhairul Akmal Abdul Basir 2020-09-25 Abdul Basir, Zulkhairul Akmal Inorganic polymers Physical and theoretical chemistry Polyvinyl chloride The composite of Polyvinylidene Fluoride/ Titanium dioxide (PVDF/TiO2) thin film were prepared with various loading of TiO2 using solvent casting method. The solution was stirred for 48 hours using magnetic stirrer at 600rpm. The mixture was casted into glass petri dish before being dried in the oven for 1 hour at 115 oC until the thin film sample formed. Then, the sample was transformed into dumbbell shape and stretched in 3 minutes. The necking area or the stretching area were studied using micrometer screw gauge, inverted microscopy, differential scanning calorimetry (DSC) and ATR-FTIR. The thickness of the thin film was increasing significantly with the addition of TiO2. Same goes to the Tensile strength, Incorporated TiO2 in the PVDF able to enhance the mechanical properties significantly. As for the surface morphology, whitening oval occurs at the control which indicates the lamella while crystal nuclide of TiO2 was formed and tend to increase with the amount TiO2 used. Next, on the DSC, the melting temperature (Tm) increased with addition of TiO2 and PVDF10 shows the highest degree of crystallinity. Lastly, on the ATR-FTIR, PVDF10 has been identified to have highest β-phase due increase the β and γ phase to the second highest peak at 1168cm-1 region, able to increase the β-phase at 1401 cm-1 and most importantly it has the highest peak on 834 cm-1 regions which indicate also the β-phase. Overall, the incorporation of PVDF10 shows the best because it able to produce highest degree of crystallinity and the β-phase. 2020-09 Thesis https://ir.uitm.edu.my/id/eprint/34665/ https://ir.uitm.edu.my/id/eprint/34665/1/34665.pdf text en public degree Universiti Teknologi Mara Perlis Faculty of Applied Sciences
institution	Universiti Teknologi MARA
collection	UiTM Institutional Repository
language	English
topic	Inorganic polymers Physical and theoretical chemistry Polyvinyl chloride
spellingShingle	Inorganic polymers Physical and theoretical chemistry Polyvinyl chloride Abdul Basir, Zulkhairul Akmal The effect of various titanium dioxide [TiO2] loading on polymorphism of stretched polyvinylidene flouride [PVDF] /TiO2 thin film / Zulkhairul Akmal Abdul Basir
description	The composite of Polyvinylidene Fluoride/ Titanium dioxide (PVDF/TiO2) thin film were prepared with various loading of TiO2 using solvent casting method. The solution was stirred for 48 hours using magnetic stirrer at 600rpm. The mixture was casted into glass petri dish before being dried in the oven for 1 hour at 115 oC until the thin film sample formed. Then, the sample was transformed into dumbbell shape and stretched in 3 minutes. The necking area or the stretching area were studied using micrometer screw gauge, inverted microscopy, differential scanning calorimetry (DSC) and ATR-FTIR. The thickness of the thin film was increasing significantly with the addition of TiO2. Same goes to the Tensile strength, Incorporated TiO2 in the PVDF able to enhance the mechanical properties significantly. As for the surface morphology, whitening oval occurs at the control which indicates the lamella while crystal nuclide of TiO2 was formed and tend to increase with the amount TiO2 used. Next, on the DSC, the melting temperature (Tm) increased with addition of TiO2 and PVDF10 shows the highest degree of crystallinity. Lastly, on the ATR-FTIR, PVDF10 has been identified to have highest β-phase due increase the β and γ phase to the second highest peak at 1168cm-1 region, able to increase the β-phase at 1401 cm-1 and most importantly it has the highest peak on 834 cm-1 regions which indicate also the β-phase. Overall, the incorporation of PVDF10 shows the best because it able to produce highest degree of crystallinity and the β-phase.
format	Thesis
qualification_level	Bachelor degree
author	Abdul Basir, Zulkhairul Akmal
author_facet	Abdul Basir, Zulkhairul Akmal
author_sort	Abdul Basir, Zulkhairul Akmal
title	The effect of various titanium dioxide [TiO2] loading on polymorphism of stretched polyvinylidene flouride [PVDF] /TiO2 thin film / Zulkhairul Akmal Abdul Basir
title_short	The effect of various titanium dioxide [TiO2] loading on polymorphism of stretched polyvinylidene flouride [PVDF] /TiO2 thin film / Zulkhairul Akmal Abdul Basir
title_full	The effect of various titanium dioxide [TiO2] loading on polymorphism of stretched polyvinylidene flouride [PVDF] /TiO2 thin film / Zulkhairul Akmal Abdul Basir
title_fullStr	The effect of various titanium dioxide [TiO2] loading on polymorphism of stretched polyvinylidene flouride [PVDF] /TiO2 thin film / Zulkhairul Akmal Abdul Basir
title_full_unstemmed	The effect of various titanium dioxide [TiO2] loading on polymorphism of stretched polyvinylidene flouride [PVDF] /TiO2 thin film / Zulkhairul Akmal Abdul Basir
title_sort	effect of various titanium dioxide [tio2] loading on polymorphism of stretched polyvinylidene flouride [pvdf] /tio2 thin film / zulkhairul akmal abdul basir
granting_institution	Universiti Teknologi Mara Perlis
granting_department	Faculty of Applied Sciences
publishDate	2020
url	https://ir.uitm.edu.my/id/eprint/34665/1/34665.pdf
_version_	1783734277599395840

The effect of various titanium dioxide [TiO2] loading on polymorphism of stretched polyvinylidene flouride [PVDF] /TiO2 thin film / Zulkhairul Akmal Abdul Basir

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