Synthesis and characterization of cerate-zirconate ceramic powder prepared by supercritical fluids, sol-gel and sol-gel assisted supercritical fluids methods: a comparison study / Najwa 'Adni Ibarahim
TGA result showed that the thermal decomposition temperature for S2 was higher than SI and S3. The traces of carbonate residue and secondary phase were observed for both S2 and S3 powder due to the incomplete combustion of intermediate compounds. However, SI shown highly crystalline powder and its X...
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2017
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my-uitm-ir.373102023-08-17T07:56:32Z Synthesis and characterization of cerate-zirconate ceramic powder prepared by supercritical fluids, sol-gel and sol-gel assisted supercritical fluids methods: a comparison study / Najwa 'Adni Ibarahim 2017 Ibarahim, Najwa 'Adni TGA result showed that the thermal decomposition temperature for S2 was higher than SI and S3. The traces of carbonate residue and secondary phase were observed for both S2 and S3 powder due to the incomplete combustion of intermediate compounds. However, SI shown highly crystalline powder and its XRD peaks were matched to the standard BCZY compound (JCPDS card 89-2485). All the major peaks can be indexed to the index miller of (110), (111), (200), (210), (220) and (310). The particle size was in the range of 0.2 to 0.5 urn for the first group of agglomerat 2017 Thesis https://ir.uitm.edu.my/id/eprint/37310/ https://ir.uitm.edu.my/id/eprint/37310/1/37310.pdf text en public masters Universiti Teknologi MARA (UiTM) Faculty of Applied Sciences Osman, Nafisah |
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Universiti Teknologi MARA |
| collection |
UiTM Institutional Repository |
| language |
English |
| advisor |
Osman, Nafisah |
| description |
TGA result showed that the thermal decomposition temperature for S2 was higher than SI and S3. The traces of carbonate residue and secondary phase were observed for both S2 and S3 powder due to the incomplete combustion of intermediate compounds. However, SI shown highly crystalline powder and its XRD peaks were matched to the standard BCZY compound (JCPDS card 89-2485). All the major peaks can be indexed to the index miller of (110), (111), (200), (210), (220) and (310). The particle size was in the range of 0.2 to 0.5 urn for the first group of agglomerat |
| format |
Thesis |
| qualification_level |
Master's degree |
| author |
Ibarahim, Najwa 'Adni |
| spellingShingle |
Ibarahim, Najwa 'Adni Synthesis and characterization of cerate-zirconate ceramic powder prepared by supercritical fluids, sol-gel and sol-gel assisted supercritical fluids methods: a comparison study / Najwa 'Adni Ibarahim |
| author_facet |
Ibarahim, Najwa 'Adni |
| author_sort |
Ibarahim, Najwa 'Adni |
| title |
Synthesis and characterization of cerate-zirconate ceramic powder prepared by supercritical fluids, sol-gel and sol-gel assisted supercritical fluids methods: a comparison study / Najwa 'Adni Ibarahim |
| title_short |
Synthesis and characterization of cerate-zirconate ceramic powder prepared by supercritical fluids, sol-gel and sol-gel assisted supercritical fluids methods: a comparison study / Najwa 'Adni Ibarahim |
| title_full |
Synthesis and characterization of cerate-zirconate ceramic powder prepared by supercritical fluids, sol-gel and sol-gel assisted supercritical fluids methods: a comparison study / Najwa 'Adni Ibarahim |
| title_fullStr |
Synthesis and characterization of cerate-zirconate ceramic powder prepared by supercritical fluids, sol-gel and sol-gel assisted supercritical fluids methods: a comparison study / Najwa 'Adni Ibarahim |
| title_full_unstemmed |
Synthesis and characterization of cerate-zirconate ceramic powder prepared by supercritical fluids, sol-gel and sol-gel assisted supercritical fluids methods: a comparison study / Najwa 'Adni Ibarahim |
| title_sort |
synthesis and characterization of cerate-zirconate ceramic powder prepared by supercritical fluids, sol-gel and sol-gel assisted supercritical fluids methods: a comparison study / najwa 'adni ibarahim |
| granting_institution |
Universiti Teknologi MARA (UiTM) |
| granting_department |
Faculty of Applied Sciences |
| publishDate |
2017 |
| url |
https://ir.uitm.edu.my/id/eprint/37310/1/37310.pdf |
| _version_ |
1783734413365870592 |