Analysis of volatile compounds from household plastic products using solid phase micro extraction (SPME) and gas chromatograph with mass spectrometry detector (GC-MSD) / Fazila Zakaria

A method for the identification of volatile compounds from some household plastic products (i.e. food packaging bag, microwaveable food container, and mineral water bottle) using solid phase microextraction (SPME) and gas chromatography with mass spectrometry detector (GC-MSD) was developed. SPME fi...

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Main Author:	Zakaria, Fazila
Format:	Thesis
Language:	English
Published:	2007
Subjects:	Indexes (General)
Online Access:	https://ir.uitm.edu.my/id/eprint/72590/1/72590.PDF
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id	my-uitm-ir.72590
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spelling	my-uitm-ir.725902023-01-15T04:15:09Z Analysis of volatile compounds from household plastic products using solid phase micro extraction (SPME) and gas chromatograph with mass spectrometry detector (GC-MSD) / Fazila Zakaria 2007-04 Zakaria, Fazila Indexes (General) A method for the identification of volatile compounds from some household plastic products (i.e. food packaging bag, microwaveable food container, and mineral water bottle) using solid phase microextraction (SPME) and gas chromatography with mass spectrometry detector (GC-MSD) was developed. SPME fiber coated with 100 urn polydimethylsiloxane was used in this study. Optimization of SPME parameters such as extraction temperature, extraction time, and desorption time on the amount of compound extracted were studied using block design and statistical software package Design-Expert 6.0.6. The optimum experimental condition was determined using response surface method. In this study, the optimized condition for SPME technique was 80°C extraction temperature, 40 minutes extraction time with desorption time of 80seconds. Using the optimized condition, the profile of volatile compounds for each type of plastic products was obtained and compared. SPME method was found to be a solvent less, rapid, and simple method in studying the profile of volatile compounds from household plastic products. 2007-04 Thesis https://ir.uitm.edu.my/id/eprint/72590/ https://ir.uitm.edu.my/id/eprint/72590/1/72590.PDF text en public degree Universiti Teknologi Mara (UiTM) Faculty of Applied Science Abdullah Munir, Zuraidah (Prof. Madya. )
institution	Universiti Teknologi MARA
collection	UiTM Institutional Repository
language	English
advisor	Abdullah Munir, Zuraidah (Prof. Madya. )
topic	Indexes (General)
spellingShingle	Indexes (General) Zakaria, Fazila Analysis of volatile compounds from household plastic products using solid phase micro extraction (SPME) and gas chromatograph with mass spectrometry detector (GC-MSD) / Fazila Zakaria
description	A method for the identification of volatile compounds from some household plastic products (i.e. food packaging bag, microwaveable food container, and mineral water bottle) using solid phase microextraction (SPME) and gas chromatography with mass spectrometry detector (GC-MSD) was developed. SPME fiber coated with 100 urn polydimethylsiloxane was used in this study. Optimization of SPME parameters such as extraction temperature, extraction time, and desorption time on the amount of compound extracted were studied using block design and statistical software package Design-Expert 6.0.6. The optimum experimental condition was determined using response surface method. In this study, the optimized condition for SPME technique was 80°C extraction temperature, 40 minutes extraction time with desorption time of 80seconds. Using the optimized condition, the profile of volatile compounds for each type of plastic products was obtained and compared. SPME method was found to be a solvent less, rapid, and simple method in studying the profile of volatile compounds from household plastic products.
format	Thesis
qualification_level	Bachelor degree
author	Zakaria, Fazila
author_facet	Zakaria, Fazila
author_sort	Zakaria, Fazila
title	Analysis of volatile compounds from household plastic products using solid phase micro extraction (SPME) and gas chromatograph with mass spectrometry detector (GC-MSD) / Fazila Zakaria
title_short	Analysis of volatile compounds from household plastic products using solid phase micro extraction (SPME) and gas chromatograph with mass spectrometry detector (GC-MSD) / Fazila Zakaria
title_full	Analysis of volatile compounds from household plastic products using solid phase micro extraction (SPME) and gas chromatograph with mass spectrometry detector (GC-MSD) / Fazila Zakaria
title_fullStr	Analysis of volatile compounds from household plastic products using solid phase micro extraction (SPME) and gas chromatograph with mass spectrometry detector (GC-MSD) / Fazila Zakaria
title_full_unstemmed	Analysis of volatile compounds from household plastic products using solid phase micro extraction (SPME) and gas chromatograph with mass spectrometry detector (GC-MSD) / Fazila Zakaria
title_sort	analysis of volatile compounds from household plastic products using solid phase micro extraction (spme) and gas chromatograph with mass spectrometry detector (gc-msd) / fazila zakaria
granting_institution	Universiti Teknologi Mara (UiTM)
granting_department	Faculty of Applied Science
publishDate	2007
url	https://ir.uitm.edu.my/id/eprint/72590/1/72590.PDF
_version_	1783735954681364480

Analysis of volatile compounds from household plastic products using solid phase micro extraction (SPME) and gas chromatograph with mass spectrometry detector (GC-MSD) / Fazila Zakaria

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