Determination of aromatic compounds in Malaysian commercialized petrol using solid phase micro extraction (SPME) coupled to gas chromatography mass spectrometry detector (GC-MSD) / Mohamad Rosdi Muhammad Razali

A method for the identification of aromatic compounds in different varieties of petrol by using solid phase microextraction (SPME) and gas chromatography-mass spectrometry detector (GC-MS) was developed. SPME fiber coated with polydimethylsiloxane (PDMS) was used in this study. The effects of import...

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Main Author: Muhammad Razali, Mohamad Rosdi
Format: Thesis
Language:English
Published: 2012
Subjects:
Online Access:https://ir.uitm.edu.my/id/eprint/74340/1/74340.PDF
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spelling my-uitm-ir.743402023-03-28T12:41:44Z Determination of aromatic compounds in Malaysian commercialized petrol using solid phase micro extraction (SPME) coupled to gas chromatography mass spectrometry detector (GC-MSD) / Mohamad Rosdi Muhammad Razali 2012-07 Muhammad Razali, Mohamad Rosdi Spectroscopy Analytical chemistry A method for the identification of aromatic compounds in different varieties of petrol by using solid phase microextraction (SPME) and gas chromatography-mass spectrometry detector (GC-MS) was developed. SPME fiber coated with polydimethylsiloxane (PDMS) was used in this study. The effects of important SPME parameters such as desorption time, extraction time and extraction temperature on the amount of compounds extracted were studied. Optimum conditions for SPME were 40°C for extraction temperature, 10 minutes for extraction time and 100 seconds for desorption time. Using the optimized conditions, aromatic compounds in different samples were determined and the benzene concentration in the samples were compared. It was found that petrol XI has the highest benzene concentration compared to other petrol samples. 2012-07 Thesis https://ir.uitm.edu.my/id/eprint/74340/ https://ir.uitm.edu.my/id/eprint/74340/1/74340.PDF text en public degree Universiti Teknologi MARA (UiTM) Faculty of Applied Science Abdullah Munir, Zuraidah
institution Universiti Teknologi MARA
collection UiTM Institutional Repository
language English
advisor Abdullah Munir, Zuraidah
topic Spectroscopy
Analytical chemistry
spellingShingle Spectroscopy
Analytical chemistry
Muhammad Razali, Mohamad Rosdi
Determination of aromatic compounds in Malaysian commercialized petrol using solid phase micro extraction (SPME) coupled to gas chromatography mass spectrometry detector (GC-MSD) / Mohamad Rosdi Muhammad Razali
description A method for the identification of aromatic compounds in different varieties of petrol by using solid phase microextraction (SPME) and gas chromatography-mass spectrometry detector (GC-MS) was developed. SPME fiber coated with polydimethylsiloxane (PDMS) was used in this study. The effects of important SPME parameters such as desorption time, extraction time and extraction temperature on the amount of compounds extracted were studied. Optimum conditions for SPME were 40°C for extraction temperature, 10 minutes for extraction time and 100 seconds for desorption time. Using the optimized conditions, aromatic compounds in different samples were determined and the benzene concentration in the samples were compared. It was found that petrol XI has the highest benzene concentration compared to other petrol samples.
format Thesis
qualification_level Bachelor degree
author Muhammad Razali, Mohamad Rosdi
author_facet Muhammad Razali, Mohamad Rosdi
author_sort Muhammad Razali, Mohamad Rosdi
title Determination of aromatic compounds in Malaysian commercialized petrol using solid phase micro extraction (SPME) coupled to gas chromatography mass spectrometry detector (GC-MSD) / Mohamad Rosdi Muhammad Razali
title_short Determination of aromatic compounds in Malaysian commercialized petrol using solid phase micro extraction (SPME) coupled to gas chromatography mass spectrometry detector (GC-MSD) / Mohamad Rosdi Muhammad Razali
title_full Determination of aromatic compounds in Malaysian commercialized petrol using solid phase micro extraction (SPME) coupled to gas chromatography mass spectrometry detector (GC-MSD) / Mohamad Rosdi Muhammad Razali
title_fullStr Determination of aromatic compounds in Malaysian commercialized petrol using solid phase micro extraction (SPME) coupled to gas chromatography mass spectrometry detector (GC-MSD) / Mohamad Rosdi Muhammad Razali
title_full_unstemmed Determination of aromatic compounds in Malaysian commercialized petrol using solid phase micro extraction (SPME) coupled to gas chromatography mass spectrometry detector (GC-MSD) / Mohamad Rosdi Muhammad Razali
title_sort determination of aromatic compounds in malaysian commercialized petrol using solid phase micro extraction (spme) coupled to gas chromatography mass spectrometry detector (gc-msd) / mohamad rosdi muhammad razali
granting_institution Universiti Teknologi MARA (UiTM)
granting_department Faculty of Applied Science
publishDate 2012
url https://ir.uitm.edu.my/id/eprint/74340/1/74340.PDF
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