Enhancement of Ta2O5 nanostructures properties via electrochemical anodization synthesis method and surface modification with gold nanoparticles for humidity sensing application / Nur Lili Suraya Ngadiman

Nanostructured metal oxide have been widely employed in electronic devices as sensing layer. One of the most crucial issue in nanostructure fabrication is to optimize the synthesis method in order to produce high sensitivity and reliable sensor. Due to this issue, a synthesis method with high potent...

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主要作者:	Ngadiman, Nur Lili Suraya
格式:	Thesis
语言:	English
出版:	2022
主题:	Nanostructured materials
在线阅读:	https://ir.uitm.edu.my/id/eprint/75746/1/75746.pdf
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id	my-uitm-ir.75746
record_format	uketd_dc
spelling	my-uitm-ir.757462023-04-04T00:43:47Z Enhancement of Ta2O5 nanostructures properties via electrochemical anodization synthesis method and surface modification with gold nanoparticles for humidity sensing application / Nur Lili Suraya Ngadiman 2022 Ngadiman, Nur Lili Suraya Nanostructured materials Detectors. Sensors. Sensor networks Nanostructured metal oxide have been widely employed in electronic devices as sensing layer. One of the most crucial issue in nanostructure fabrication is to optimize the synthesis method in order to produce high sensitivity and reliable sensor. Due to this issue, a synthesis method with high potential to produce metal oxide nanostructures on tantalum foil substrate, namely anodization, is highlighted in this study and surface modification using doped gold nanoparticles is also implemented to improve the characteristics of the nanostructured sensing layer. A set of parameter has been optimized to synthesis Tantalum Pentoxide (Ta2O5) via anodization synthesis method. Anodization is one of the simplest synthesis methods for fabricating generous nanostructures metal oxide. The purpose of this study is to optimize the anodization time and voltage of Ta2O5, employ the optimized Ta2O5 as humidity sensor and improve the functionality through doping method. The significant growth of anodized Ta2O5 nanotubes has increased the number of pore structures and offered more water absorption active sites for humidity sensing detection. Physical and chemical properties of anodized Ta2O5 nanotubes were justified using FESEM, XRD, EDX, AFM and UVVIS analysis. Synthesizing nanostructures through anodization method producing Ta2O5 nanotubes with pore diameter ranging between 10 to 50 nm. From XRD analysis, cubic crystalline structure was obtained through annealing at 500 °C for 2 hours, thus improved its crystalline structure and generated a favourable medium of interaction. 2022 Thesis https://ir.uitm.edu.my/id/eprint/75746/ https://ir.uitm.edu.my/id/eprint/75746/1/75746.pdf text en public masters Universiti Teknologi MARA (UiTM) College of Engineering Abdul Rani, Rozina
institution	Universiti Teknologi MARA
collection	UiTM Institutional Repository
language	English
advisor	Abdul Rani, Rozina
topic	Nanostructured materials Nanostructured materials
spellingShingle	Nanostructured materials Nanostructured materials Ngadiman, Nur Lili Suraya Enhancement of Ta2O5 nanostructures properties via electrochemical anodization synthesis method and surface modification with gold nanoparticles for humidity sensing application / Nur Lili Suraya Ngadiman
description	Nanostructured metal oxide have been widely employed in electronic devices as sensing layer. One of the most crucial issue in nanostructure fabrication is to optimize the synthesis method in order to produce high sensitivity and reliable sensor. Due to this issue, a synthesis method with high potential to produce metal oxide nanostructures on tantalum foil substrate, namely anodization, is highlighted in this study and surface modification using doped gold nanoparticles is also implemented to improve the characteristics of the nanostructured sensing layer. A set of parameter has been optimized to synthesis Tantalum Pentoxide (Ta2O5) via anodization synthesis method. Anodization is one of the simplest synthesis methods for fabricating generous nanostructures metal oxide. The purpose of this study is to optimize the anodization time and voltage of Ta2O5, employ the optimized Ta2O5 as humidity sensor and improve the functionality through doping method. The significant growth of anodized Ta2O5 nanotubes has increased the number of pore structures and offered more water absorption active sites for humidity sensing detection. Physical and chemical properties of anodized Ta2O5 nanotubes were justified using FESEM, XRD, EDX, AFM and UVVIS analysis. Synthesizing nanostructures through anodization method producing Ta2O5 nanotubes with pore diameter ranging between 10 to 50 nm. From XRD analysis, cubic crystalline structure was obtained through annealing at 500 °C for 2 hours, thus improved its crystalline structure and generated a favourable medium of interaction.
format	Thesis
qualification_level	Master's degree
author	Ngadiman, Nur Lili Suraya
author_facet	Ngadiman, Nur Lili Suraya
author_sort	Ngadiman, Nur Lili Suraya
title	Enhancement of Ta2O5 nanostructures properties via electrochemical anodization synthesis method and surface modification with gold nanoparticles for humidity sensing application / Nur Lili Suraya Ngadiman
title_short	Enhancement of Ta2O5 nanostructures properties via electrochemical anodization synthesis method and surface modification with gold nanoparticles for humidity sensing application / Nur Lili Suraya Ngadiman
title_full	Enhancement of Ta2O5 nanostructures properties via electrochemical anodization synthesis method and surface modification with gold nanoparticles for humidity sensing application / Nur Lili Suraya Ngadiman
title_fullStr	Enhancement of Ta2O5 nanostructures properties via electrochemical anodization synthesis method and surface modification with gold nanoparticles for humidity sensing application / Nur Lili Suraya Ngadiman
title_full_unstemmed	Enhancement of Ta2O5 nanostructures properties via electrochemical anodization synthesis method and surface modification with gold nanoparticles for humidity sensing application / Nur Lili Suraya Ngadiman
title_sort	enhancement of ta2o5 nanostructures properties via electrochemical anodization synthesis method and surface modification with gold nanoparticles for humidity sensing application / nur lili suraya ngadiman
granting_institution	Universiti Teknologi MARA (UiTM)
granting_department	College of Engineering
publishDate	2022
url	https://ir.uitm.edu.my/id/eprint/75746/1/75746.pdf
_version_	1783736079136849920

Enhancement of Ta2O5 nanostructures properties via electrochemical anodization synthesis method and surface modification with gold nanoparticles for humidity sensing application / Nur Lili Suraya Ngadiman

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