Preparation of iron electrode derived from iron steel waste for decolorization of various type of dyes via electrocoagulation method / Nurul Athikah Azizan

This present study examines the preparation of iron electrode (Fe.S) derived from iron steel waste for decolorization of Reactive Black 5 (RB5), Acid Blue 29 (AB29), and Methylene Blue (MB) via electrocoagulation method. The Fe.S was synthesized by varying the loading of iron steel waste and Polytet...

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Main Author:	Azizan, Nurul Athikah
Format:	Thesis
Language:	English
Published:	2023
Subjects:	Electrochemical analysis
Online Access:	https://ir.uitm.edu.my/id/eprint/88753/1/88753.pdf
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id	my-uitm-ir.88753
record_format	uketd_dc
spelling	my-uitm-ir.887532024-01-02T02:17:52Z Preparation of iron electrode derived from iron steel waste for decolorization of various type of dyes via electrocoagulation method / Nurul Athikah Azizan 2023 Azizan, Nurul Athikah Electrochemical analysis TA Engineering. Civil engineering This present study examines the preparation of iron electrode (Fe.S) derived from iron steel waste for decolorization of Reactive Black 5 (RB5), Acid Blue 29 (AB29), and Methylene Blue (MB) via electrocoagulation method. The Fe.S was synthesized by varying the loading of iron steel waste and Polytetrafluoroethylene (PTFE) as binder. The Fe.S electrode was characterized using Scanning Electron Microscopy-Energy Dispersive X-ray (SEM-EDX), nitrogen adsorption analysis, X-ray Fluorescence Spectrometer (XRF), and Fourier Transformed Infra-red (FTIR). Additionally, electrochemical characterisation was executed using cyclic voltammetry (CV) and potential electrochemical impedance spectroscopy (PEIS). The electrodes performance was assessed at different operating parameters which includes initial pH, current density, and initial dye concentration. Subsequently, the stability of the Fe.S electrode was tested for the best operating conditions. The best preparation iron electrode was found at 3 g of iron sludge powder loading and 30 wt% of PTFE as binder at ratio 4:1:3, denoted as 30Fe.S which exhibited almost complete decolorization within 60 minutes of treatment time. Interestingly, the best preparation iron electrode also has minimum chemical oxygen demand (COD) of 67% compared to others composition loading ratio. 2023 Thesis https://ir.uitm.edu.my/id/eprint/88753/ https://ir.uitm.edu.my/id/eprint/88753/1/88753.pdf text en public masters Universiti Teknologi MARA (UiTM) College of Engineering -, Norhaslinda Nasuha
institution	Universiti Teknologi MARA
collection	UiTM Institutional Repository
language	English
advisor	-, Norhaslinda Nasuha
topic	Electrochemical analysis Electrochemical analysis
spellingShingle	Electrochemical analysis Electrochemical analysis Azizan, Nurul Athikah Preparation of iron electrode derived from iron steel waste for decolorization of various type of dyes via electrocoagulation method / Nurul Athikah Azizan
description	This present study examines the preparation of iron electrode (Fe.S) derived from iron steel waste for decolorization of Reactive Black 5 (RB5), Acid Blue 29 (AB29), and Methylene Blue (MB) via electrocoagulation method. The Fe.S was synthesized by varying the loading of iron steel waste and Polytetrafluoroethylene (PTFE) as binder. The Fe.S electrode was characterized using Scanning Electron Microscopy-Energy Dispersive X-ray (SEM-EDX), nitrogen adsorption analysis, X-ray Fluorescence Spectrometer (XRF), and Fourier Transformed Infra-red (FTIR). Additionally, electrochemical characterisation was executed using cyclic voltammetry (CV) and potential electrochemical impedance spectroscopy (PEIS). The electrodes performance was assessed at different operating parameters which includes initial pH, current density, and initial dye concentration. Subsequently, the stability of the Fe.S electrode was tested for the best operating conditions. The best preparation iron electrode was found at 3 g of iron sludge powder loading and 30 wt% of PTFE as binder at ratio 4:1:3, denoted as 30Fe.S which exhibited almost complete decolorization within 60 minutes of treatment time. Interestingly, the best preparation iron electrode also has minimum chemical oxygen demand (COD) of 67% compared to others composition loading ratio.
format	Thesis
qualification_level	Master's degree
author	Azizan, Nurul Athikah
author_facet	Azizan, Nurul Athikah
author_sort	Azizan, Nurul Athikah
title	Preparation of iron electrode derived from iron steel waste for decolorization of various type of dyes via electrocoagulation method / Nurul Athikah Azizan
title_short	Preparation of iron electrode derived from iron steel waste for decolorization of various type of dyes via electrocoagulation method / Nurul Athikah Azizan
title_full	Preparation of iron electrode derived from iron steel waste for decolorization of various type of dyes via electrocoagulation method / Nurul Athikah Azizan
title_fullStr	Preparation of iron electrode derived from iron steel waste for decolorization of various type of dyes via electrocoagulation method / Nurul Athikah Azizan
title_full_unstemmed	Preparation of iron electrode derived from iron steel waste for decolorization of various type of dyes via electrocoagulation method / Nurul Athikah Azizan
title_sort	preparation of iron electrode derived from iron steel waste for decolorization of various type of dyes via electrocoagulation method / nurul athikah azizan
granting_institution	Universiti Teknologi MARA (UiTM)
granting_department	College of Engineering
publishDate	2023
url	https://ir.uitm.edu.my/id/eprint/88753/1/88753.pdf
_version_	1794192154493452288

Preparation of iron electrode derived from iron steel waste for decolorization of various type of dyes via electrocoagulation method / Nurul Athikah Azizan

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