Synthesis, characterization and catalytic study of functionalized polymer supported palladium(II) hydrazone complexes containing electron donating group as catalysts in heck reaction / Najwa Asilah M Shamsuddin

Synthesis, characterization and catalytic study of functionalized polymer supported palladium(II) hydrazone complexes containing electron donating group as catalysts in heck reaction / Najwa Asilah M Shamsuddin

Heck reaction was discovered as one of the cross-coupling reactions where the coupling occurs between aryl halides and alkenes that using palladium as catalyst. Immobilization of catalysts on insoluble supports which is chloromethylated polystyrene or Merrifield resin have been expected as best subs...

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Main Author: M Shamsuddin, Najwa Asilah
Format: Thesis
Language:English
Published: 2023
Online Access:https://ir.uitm.edu.my/id/eprint/88786/1/88786.pdf
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spelling my-uitm-ir.887862023-12-26T07:37:21Z Synthesis, characterization and catalytic study of functionalized polymer supported palladium(II) hydrazone complexes containing electron donating group as catalysts in heck reaction / Najwa Asilah M Shamsuddin 2023 M Shamsuddin, Najwa Asilah Heck reaction was discovered as one of the cross-coupling reactions where the coupling occurs between aryl halides and alkenes that using palladium as catalyst. Immobilization of catalysts on insoluble supports which is chloromethylated polystyrene or Merrifield resin have been expected as best substitutes to soluble polymer supports due to inert, non-toxic, and non-volatile characteristics. Thus, this study reports on the synthesis and characterization of functionalized polystyrene-supported palladium(II)-hydrazone complexes containing electron donating group (-OH and -CH3) and their catalytic behaviour for Heck reaction. The first step of synthesis began with aldehyde functionalization of chloromethylated polystyrene to form PS-CHO. 2023 Thesis https://ir.uitm.edu.my/id/eprint/88786/ https://ir.uitm.edu.my/id/eprint/88786/1/88786.pdf text en public masters Universiti Teknologi MARA (UiTM) Faculty of Applied Sciences Said, Nur Rahimah
institution Universiti Teknologi MARA
collection UiTM Institutional Repository
language English
advisor Said, Nur Rahimah
description Heck reaction was discovered as one of the cross-coupling reactions where the coupling occurs between aryl halides and alkenes that using palladium as catalyst. Immobilization of catalysts on insoluble supports which is chloromethylated polystyrene or Merrifield resin have been expected as best substitutes to soluble polymer supports due to inert, non-toxic, and non-volatile characteristics. Thus, this study reports on the synthesis and characterization of functionalized polystyrene-supported palladium(II)-hydrazone complexes containing electron donating group (-OH and -CH3) and their catalytic behaviour for Heck reaction. The first step of synthesis began with aldehyde functionalization of chloromethylated polystyrene to form PS-CHO.
format Thesis
qualification_level Master's degree
author M Shamsuddin, Najwa Asilah
spellingShingle M Shamsuddin, Najwa Asilah
Synthesis, characterization and catalytic study of functionalized polymer supported palladium(II) hydrazone complexes containing electron donating group as catalysts in heck reaction / Najwa Asilah M Shamsuddin
author_facet M Shamsuddin, Najwa Asilah
author_sort M Shamsuddin, Najwa Asilah
title Synthesis, characterization and catalytic study of functionalized polymer supported palladium(II) hydrazone complexes containing electron donating group as catalysts in heck reaction / Najwa Asilah M Shamsuddin
title_short Synthesis, characterization and catalytic study of functionalized polymer supported palladium(II) hydrazone complexes containing electron donating group as catalysts in heck reaction / Najwa Asilah M Shamsuddin
title_full Synthesis, characterization and catalytic study of functionalized polymer supported palladium(II) hydrazone complexes containing electron donating group as catalysts in heck reaction / Najwa Asilah M Shamsuddin
title_fullStr Synthesis, characterization and catalytic study of functionalized polymer supported palladium(II) hydrazone complexes containing electron donating group as catalysts in heck reaction / Najwa Asilah M Shamsuddin
title_full_unstemmed Synthesis, characterization and catalytic study of functionalized polymer supported palladium(II) hydrazone complexes containing electron donating group as catalysts in heck reaction / Najwa Asilah M Shamsuddin
title_sort synthesis, characterization and catalytic study of functionalized polymer supported palladium(ii) hydrazone complexes containing electron donating group as catalysts in heck reaction / najwa asilah m shamsuddin
granting_institution Universiti Teknologi MARA (UiTM)
granting_department Faculty of Applied Sciences
publishDate 2023
url https://ir.uitm.edu.my/id/eprint/88786/1/88786.pdf
_version_ 1794192161356382208

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