Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa
The synthesis of 4-allyoxy-11, 13-dimethoxystilbene has been made using a series of reactions. Protected iodophenol reaction was the first step using allyl bromide as a protecting agent. After that, through Wittig reaction the protected styrene was successfully synthesized. Both compound finally wer...
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| Language: | English |
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2005
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| Online Access: | https://ir.uitm.edu.my/id/eprint/98485/1/98485.PDF |
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my-uitm-ir.984852024-08-27T18:11:44Z Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa 2005 Che Pa, Mohd Farizh QD Chemistry RM Therapeutics. Pharmacology The synthesis of 4-allyoxy-11, 13-dimethoxystilbene has been made using a series of reactions. Protected iodophenol reaction was the first step using allyl bromide as a protecting agent. After that, through Wittig reaction the protected styrene was successfully synthesized. Both compound finally were coupled in the presence of palladium chloride as a catalyst and triphenylphospine as a ligand via Heck reaction to give about 28.84% yield. TLC, UV spectrophotometer and NMR spectrometer were used in the determination of every product for every step. However, the desired compound, which is expected to be formed, was not successfully synthesized due to unknown reason. 2005 Thesis https://ir.uitm.edu.my/id/eprint/98485/ https://ir.uitm.edu.my/id/eprint/98485/1/98485.PDF text en public degree Universiti Teknologi MARA (Kampus Puncak Alam) Faculty of Pharmacy Abdul Wahab, Ibtisam |
| institution |
Universiti Teknologi MARA |
| collection |
UiTM Institutional Repository |
| language |
English |
| advisor |
Abdul Wahab, Ibtisam |
| topic |
QD Chemistry QD Chemistry |
| spellingShingle |
QD Chemistry QD Chemistry Che Pa, Mohd Farizh Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa |
| description |
The synthesis of 4-allyoxy-11, 13-dimethoxystilbene has been made using a series of reactions. Protected iodophenol reaction was the first step using allyl bromide as a protecting agent. After that, through Wittig reaction the protected styrene was successfully synthesized. Both compound finally were coupled in the presence of palladium chloride as a catalyst and triphenylphospine as a ligand via Heck reaction to give about 28.84% yield. TLC, UV spectrophotometer and NMR spectrometer were used in the determination of every product for every step. However, the desired compound, which is expected to be formed, was not successfully synthesized due to unknown reason. |
| format |
Thesis |
| qualification_level |
Bachelor degree |
| author |
Che Pa, Mohd Farizh |
| author_facet |
Che Pa, Mohd Farizh |
| author_sort |
Che Pa, Mohd Farizh |
| title |
Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa |
| title_short |
Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa |
| title_full |
Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa |
| title_fullStr |
Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa |
| title_full_unstemmed |
Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa |
| title_sort |
synthesis of 4-allyloxy-11, 13-dimethoxystilbene / mohd farizh che pa |
| granting_institution |
Universiti Teknologi MARA (Kampus Puncak Alam) |
| granting_department |
Faculty of Pharmacy |
| publishDate |
2005 |
| url |
https://ir.uitm.edu.my/id/eprint/98485/1/98485.PDF |
| _version_ |
1811768925908631552 |