Synthesis and Characterization of Carbon Nanodots for Detection and Quantification of Ferric (III) Ions
In this research, green electrochemically synthesized Carbon Nanodots (C-Dots) and one-pot microwave synthesized Nitrogen-doped Carbon Nanodots (N-CDs) were studied as chemical sensor for detection of Ferric (Fe3+) ions. C-Dots were synthesized electrochemically through a green chemistry approach us...
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my-unimas-ir.211572023-08-23T06:22:49Z Synthesis and Characterization of Carbon Nanodots for Detection and Quantification of Ferric (III) Ions 2017 Tan, Shao Chien Q Science (General) QC Physics QD Chemistry In this research, green electrochemically synthesized Carbon Nanodots (C-Dots) and one-pot microwave synthesized Nitrogen-doped Carbon Nanodots (N-CDs) were studied as chemical sensor for detection of Ferric (Fe3+) ions. C-Dots were synthesized electrochemically through a green chemistry approach using spent battery carbon rods and ultrapure water. The C-Dots were used to modify Screen Printed Carbon Electrode (SPCE) through drop-coating method and the electrochemical properties were characterized using Cyclic Voltammetry (CV). The current intensity of the C-Dots modified SPCE was shown to improve significantly by 259% when compared to the unmodified SPCE. Various concentration of Fe3+ ions ranging from 0.5 to 25.0 ppm further enhanced the current intensity up to 734% when compared with unmodified SPCE, showing a trend of linear relationship. The SPCE electrochemical sensor strip exhibited a linear detection range of 0.5 to 25.0 ppm Fe3+ ions and the limit of detection (LOD) calculated was 0.44 ± 0.04 ppm (S/N ratio of 3). unimas 2017 Thesis http://ir.unimas.my/id/eprint/21157/ http://ir.unimas.my/id/eprint/21157/1/Shao%20Chien.pdf text en validuser masters UNIMAS |
| institution |
Universiti Malaysia Sarawak |
| collection |
UNIMAS Institutional Repository |
| language |
English |
| topic |
Q Science (General) QC Physics QD Chemistry |
| spellingShingle |
Q Science (General) QC Physics QD Chemistry Tan, Shao Chien Synthesis and Characterization of Carbon Nanodots for Detection and Quantification of Ferric (III) Ions |
| description |
In this research, green electrochemically synthesized Carbon Nanodots (C-Dots) and one-pot microwave synthesized Nitrogen-doped Carbon Nanodots (N-CDs) were studied as chemical sensor for detection of Ferric (Fe3+) ions. C-Dots were synthesized electrochemically through a green chemistry approach using spent battery carbon rods and ultrapure water. The C-Dots were used to modify Screen Printed Carbon Electrode (SPCE) through drop-coating method
and the electrochemical properties were characterized using Cyclic Voltammetry (CV). The
current intensity of the C-Dots modified SPCE was shown to improve significantly by 259% when compared to the unmodified SPCE. Various concentration of Fe3+ ions ranging from 0.5 to 25.0 ppm further enhanced the current intensity up to 734% when compared with unmodified SPCE, showing a trend of linear relationship. The SPCE electrochemical sensor strip exhibited a linear detection range of 0.5 to 25.0 ppm Fe3+ ions and the limit of detection (LOD) calculated was 0.44 ± 0.04 ppm (S/N ratio of 3). |
| format |
Thesis |
| qualification_level |
Master's degree |
| author |
Tan, Shao Chien |
| author_facet |
Tan, Shao Chien |
| author_sort |
Tan, Shao Chien |
| title |
Synthesis and Characterization of Carbon Nanodots for Detection and Quantification of Ferric (III) Ions |
| title_short |
Synthesis and Characterization of Carbon Nanodots for Detection and Quantification of Ferric (III) Ions |
| title_full |
Synthesis and Characterization of Carbon Nanodots for Detection and Quantification of Ferric (III) Ions |
| title_fullStr |
Synthesis and Characterization of Carbon Nanodots for Detection and Quantification of Ferric (III) Ions |
| title_full_unstemmed |
Synthesis and Characterization of Carbon Nanodots for Detection and Quantification of Ferric (III) Ions |
| title_sort |
synthesis and characterization of carbon nanodots for detection and quantification of ferric (iii) ions |
| granting_institution |
UNIMAS |
| publishDate |
2017 |
| url |
http://ir.unimas.my/id/eprint/21157/1/Shao%20Chien.pdf |
| _version_ |
1783728226887008256 |