Electrophoretic Deposition of Carbon Nanotubes onto Carbon Fiber Laminated Composites: Effect of Suspension Medium, Deposition Voltage, and Time

Multiwalled carbon nanotubes-Carbon Fiber (MWCNT–CF/) epoxy laminated composites are widely used in many applications, and electrophoretic deposition (EPD) is a hybridisation method that is often used. This research focuses on improving the technique by optimising the input parameters to obtain comp...

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Main Author: Nur-Azzah Afifah, Taib
Format: Thesis
Language:English
English
English
Published: 2023
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Online Access:http://ir.unimas.my/id/eprint/43454/3/Nur.Azzah_dsva.pdf
http://ir.unimas.my/id/eprint/43454/4/Thesis%20Master%20Nor%20Azzah%20-%2024pages.pdf
http://ir.unimas.my/id/eprint/43454/5/Thesis%20Master%20Nor%20Azzah.ftext.pdf
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spelling my-unimas-ir.434542023-12-26T04:32:56Z Electrophoretic Deposition of Carbon Nanotubes onto Carbon Fiber Laminated Composites: Effect of Suspension Medium, Deposition Voltage, and Time 2023-11-28 Nur-Azzah Afifah, Taib TP Chemical technology Multiwalled carbon nanotubes-Carbon Fiber (MWCNT–CF/) epoxy laminated composites are widely used in many applications, and electrophoretic deposition (EPD) is a hybridisation method that is often used. This research focuses on improving the technique by optimising the input parameters to obtain composites with enhanced tensile properties. Various studies have utilized the EPD method, but there hardly any study utilized the water-methanol mixture as the medium. This study showed that the input parameters (volume ratio of suspension medium, deposition voltage, and time) influenced the responses of the research (tensile strength and Young’s modulus). Firstly, the optical observation showed good distribution of MWCNTs throughout the medium. Secondly, the analyses of Fourier Transform Infra-Red (FTIR), Scanning Electron Microscopy (SEM), and tensile properties demonstrated that the input factors directly influenced the composites. Thirdly, the ideal factors that correspond to the desired responses were obtained through the optimization. For the first design of experiment (DoE) (0% water, 100% methanol and 100% water,0% methanol), the optimum conditions were a volume ratio of 99.99% water, a voltage of 20V, and time of 8.88 minutes, producing maximum tensile strength and young’s modulus of 7.983 N/mm2 and 268.558 N/mm2, respectively. For the second DoE (20% water,80% methanol and 80% water, 20% methanol), tensile strength and young’s modulus of 7.2766 N/mm2 and 266.78 N/mm2, respectively, were achieved when the ideal conditions were: volume ratio of 79.99 % water, voltage of 20V, and time of 5.22 minutes. Keywords: MWCNTs, CF, epoxy, EPD, tensile properties Universiti Malaysia Sarawak 2023-11 Thesis http://ir.unimas.my/id/eprint/43454/ http://ir.unimas.my/id/eprint/43454/3/Nur.Azzah_dsva.pdf text en staffonly http://ir.unimas.my/id/eprint/43454/4/Thesis%20Master%20Nor%20Azzah%20-%2024pages.pdf text en public http://ir.unimas.my/id/eprint/43454/5/Thesis%20Master%20Nor%20Azzah.ftext.pdf text en validuser masters Faculty of Engineering Chemical Engineering
institution Universiti Malaysia Sarawak
collection UNIMAS Institutional Repository
language English
English
English
topic TP Chemical technology
spellingShingle TP Chemical technology
Nur-Azzah Afifah, Taib
Electrophoretic Deposition of Carbon Nanotubes onto Carbon Fiber Laminated Composites: Effect of Suspension Medium, Deposition Voltage, and Time
description Multiwalled carbon nanotubes-Carbon Fiber (MWCNT–CF/) epoxy laminated composites are widely used in many applications, and electrophoretic deposition (EPD) is a hybridisation method that is often used. This research focuses on improving the technique by optimising the input parameters to obtain composites with enhanced tensile properties. Various studies have utilized the EPD method, but there hardly any study utilized the water-methanol mixture as the medium. This study showed that the input parameters (volume ratio of suspension medium, deposition voltage, and time) influenced the responses of the research (tensile strength and Young’s modulus). Firstly, the optical observation showed good distribution of MWCNTs throughout the medium. Secondly, the analyses of Fourier Transform Infra-Red (FTIR), Scanning Electron Microscopy (SEM), and tensile properties demonstrated that the input factors directly influenced the composites. Thirdly, the ideal factors that correspond to the desired responses were obtained through the optimization. For the first design of experiment (DoE) (0% water, 100% methanol and 100% water,0% methanol), the optimum conditions were a volume ratio of 99.99% water, a voltage of 20V, and time of 8.88 minutes, producing maximum tensile strength and young’s modulus of 7.983 N/mm2 and 268.558 N/mm2, respectively. For the second DoE (20% water,80% methanol and 80% water, 20% methanol), tensile strength and young’s modulus of 7.2766 N/mm2 and 266.78 N/mm2, respectively, were achieved when the ideal conditions were: volume ratio of 79.99 % water, voltage of 20V, and time of 5.22 minutes. Keywords: MWCNTs, CF, epoxy, EPD, tensile properties
format Thesis
qualification_level Master's degree
author Nur-Azzah Afifah, Taib
author_facet Nur-Azzah Afifah, Taib
author_sort Nur-Azzah Afifah, Taib
title Electrophoretic Deposition of Carbon Nanotubes onto Carbon Fiber Laminated Composites: Effect of Suspension Medium, Deposition Voltage, and Time
title_short Electrophoretic Deposition of Carbon Nanotubes onto Carbon Fiber Laminated Composites: Effect of Suspension Medium, Deposition Voltage, and Time
title_full Electrophoretic Deposition of Carbon Nanotubes onto Carbon Fiber Laminated Composites: Effect of Suspension Medium, Deposition Voltage, and Time
title_fullStr Electrophoretic Deposition of Carbon Nanotubes onto Carbon Fiber Laminated Composites: Effect of Suspension Medium, Deposition Voltage, and Time
title_full_unstemmed Electrophoretic Deposition of Carbon Nanotubes onto Carbon Fiber Laminated Composites: Effect of Suspension Medium, Deposition Voltage, and Time
title_sort electrophoretic deposition of carbon nanotubes onto carbon fiber laminated composites: effect of suspension medium, deposition voltage, and time
granting_institution Faculty of Engineering
granting_department Chemical Engineering
publishDate 2023
url http://ir.unimas.my/id/eprint/43454/3/Nur.Azzah_dsva.pdf
http://ir.unimas.my/id/eprint/43454/4/Thesis%20Master%20Nor%20Azzah%20-%2024pages.pdf
http://ir.unimas.my/id/eprint/43454/5/Thesis%20Master%20Nor%20Azzah.ftext.pdf
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