Synthesis And Characterization Of Nanocomposite: 2-4-Dichlorophenoxy Acetate-Zinc-Aluminium Hydrotalcitelike Layers

A direct intercalation of 2,4-dichlorophenoxyacetate (2,4-D) into Zn-Al-Iayered double hydroxide (ZAL) was carried out by spontaneous self-assembly technique to produce Zn- AI-2,4-D nanocomposite (ZAD). The aging process was done by conventional and microwave-assisted methods. For both methods, t...

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Main Author:	Mohd Amin, Junainah
Format:	Thesis
Language:	English English
Published:	2003
Subjects:	Nanostructured materials
Online Access:	http://psasir.upm.edu.my/id/eprint/11670/1/FSAS_2003_44_A.pdf
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id	my-upm-ir.11670
record_format	uketd_dc
spelling	my-upm-ir.116702012-05-22T03:06:00Z Synthesis And Characterization Of Nanocomposite: 2-4-Dichlorophenoxy Acetate-Zinc-Aluminium Hydrotalcitelike Layers 2003-09 Mohd Amin, Junainah A direct intercalation of 2,4-dichlorophenoxyacetate (2,4-D) into Zn-Al-Iayered double hydroxide (ZAL) was carried out by spontaneous self-assembly technique to produce Zn- AI-2,4-D nanocomposite (ZAD). The aging process was done by conventional and microwave-assisted methods. For both methods, the results showed that the intercalation process resulted in the expansion of the interlayer spacing from 10.7 A in ZAL to around 19.0 - 24.6 A in ZAD. Sharp and intense peaks for 003 and 006 reflections indicate wellordered layered structure which exhibit some common features of layered materials, e.g. narrow, symmetrical and strong peaks at low 20values and weaker, less symmetric peaks at higher 20 values. Further characterization of the resulting materials including organicinorganic content, surface area and porosity, thermal analysis and morphology, were also carried out. Nanostructured materials 2003-09 Thesis http://psasir.upm.edu.my/id/eprint/11670/ http://psasir.upm.edu.my/id/eprint/11670/1/FSAS_2003_44_A.pdf application/pdf en public masters Universiti Putra Malaysia Nanostructured materials Faculty of Environmental studies English
institution	Universiti Putra Malaysia
collection	PSAS Institutional Repository
language	English English
topic	Nanostructured materials
spellingShingle	Nanostructured materials Mohd Amin, Junainah Synthesis And Characterization Of Nanocomposite: 2-4-Dichlorophenoxy Acetate-Zinc-Aluminium Hydrotalcitelike Layers
description	A direct intercalation of 2,4-dichlorophenoxyacetate (2,4-D) into Zn-Al-Iayered double hydroxide (ZAL) was carried out by spontaneous self-assembly technique to produce Zn- AI-2,4-D nanocomposite (ZAD). The aging process was done by conventional and microwave-assisted methods. For both methods, the results showed that the intercalation process resulted in the expansion of the interlayer spacing from 10.7 A in ZAL to around 19.0 - 24.6 A in ZAD. Sharp and intense peaks for 003 and 006 reflections indicate wellordered layered structure which exhibit some common features of layered materials, e.g. narrow, symmetrical and strong peaks at low 20values and weaker, less symmetric peaks at higher 20 values. Further characterization of the resulting materials including organicinorganic content, surface area and porosity, thermal analysis and morphology, were also carried out.
format	Thesis
qualification_level	Master's degree
author	Mohd Amin, Junainah
author_facet	Mohd Amin, Junainah
author_sort	Mohd Amin, Junainah
title	Synthesis And Characterization Of Nanocomposite: 2-4-Dichlorophenoxy Acetate-Zinc-Aluminium Hydrotalcitelike Layers
title_short	Synthesis And Characterization Of Nanocomposite: 2-4-Dichlorophenoxy Acetate-Zinc-Aluminium Hydrotalcitelike Layers
title_full	Synthesis And Characterization Of Nanocomposite: 2-4-Dichlorophenoxy Acetate-Zinc-Aluminium Hydrotalcitelike Layers
title_fullStr	Synthesis And Characterization Of Nanocomposite: 2-4-Dichlorophenoxy Acetate-Zinc-Aluminium Hydrotalcitelike Layers
title_full_unstemmed	Synthesis And Characterization Of Nanocomposite: 2-4-Dichlorophenoxy Acetate-Zinc-Aluminium Hydrotalcitelike Layers
title_sort	synthesis and characterization of nanocomposite: 2-4-dichlorophenoxy acetate-zinc-aluminium hydrotalcitelike layers
granting_institution	Universiti Putra Malaysia
granting_department	Faculty of Environmental studies
publishDate	2003
url	http://psasir.upm.edu.my/id/eprint/11670/1/FSAS_2003_44_A.pdf
_version_	1747811249721180160

Synthesis And Characterization Of Nanocomposite: 2-4-Dichlorophenoxy Acetate-Zinc-Aluminium Hydrotalcitelike Layers

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