Enzymatic Synthesis of Palm Based Fatty Monoethanolamide
Fatty monoethanolamides, derived from a reaction between triglyceride, palm kernel olein (PKL) or free fatty acids and primary amine alcohol, monoethanolamine (MEA) can be synthesised enzymatically, under milder conditions than the energy intensive chemical reaction. Mixture of palm based fatty m...
Saved in:
Main Author: | |
---|---|
Format: | Thesis |
Language: | English English |
Published: |
2002
|
Subjects: | |
Online Access: | http://psasir.upm.edu.my/id/eprint/9523/1/FSAS_2002_53.pdf |
Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
id |
my-upm-ir.9523 |
---|---|
record_format |
uketd_dc |
spelling |
my-upm-ir.95232024-03-06T08:49:53Z Enzymatic Synthesis of Palm Based Fatty Monoethanolamide 2002-07 Abdul Rahim, Rashidah Fatty monoethanolamides, derived from a reaction between triglyceride, palm kernel olein (PKL) or free fatty acids and primary amine alcohol, monoethanolamine (MEA) can be synthesised enzymatically, under milder conditions than the energy intensive chemical reaction. Mixture of palm based fatty monoethanolamide was successfully obtained from the reaction between PKL and MEA in the presence of enzyme with better yield than the control experiment (without enzyme). The various individual fatty monoethanolamides were also obtained from the reaction between free fatty acids (ClOCIS) and MEA after the isolation and purification processes. The various fatty monoethanolamides were used as standards for the analysis of product mixture. Fatty monoethanolamides were characterised by infra-red spectroscopy (IR), thin-layer chromatography (TLC), nuclear magnetic resonance (NMR) and gas chromatography (GC). Gas chromatograph was also used for the quantitative analysis to calculate percent yield by using internal standard method. 2002-07 Thesis http://psasir.upm.edu.my/id/eprint/9523/ http://psasir.upm.edu.my/id/eprint/9523/1/FSAS_2002_53.pdf text en public doctoral Universiti Putra Malaysia Faculty of Science and Environmental Studies Salleh, Abu Bakar English |
institution |
Universiti Putra Malaysia |
collection |
PSAS Institutional Repository |
language |
English English |
advisor |
Salleh, Abu Bakar |
topic |
|
spellingShingle |
Abdul Rahim, Rashidah Enzymatic Synthesis of Palm Based Fatty Monoethanolamide |
description |
Fatty monoethanolamides, derived from a reaction between triglyceride, palm kernel
olein (PKL) or free fatty acids and primary amine alcohol, monoethanolamine (MEA)
can be synthesised enzymatically, under milder conditions than the energy intensive
chemical reaction. Mixture of palm based fatty monoethanolamide was successfully
obtained from the reaction between PKL and MEA in the presence of enzyme with
better yield than the control experiment (without enzyme). The various individual fatty
monoethanolamides were also obtained from the reaction between free fatty acids (ClOCIS)
and MEA after the isolation and purification processes. The various fatty
monoethanolamides were used as standards for the analysis of product mixture.
Fatty monoethanolamides were characterised by infra-red spectroscopy (IR), thin-layer
chromatography (TLC), nuclear magnetic resonance (NMR) and gas chromatography (GC). Gas chromatograph was also used for the quantitative analysis to calculate percent
yield by using internal standard method. |
format |
Thesis |
qualification_level |
Doctorate |
author |
Abdul Rahim, Rashidah |
author_facet |
Abdul Rahim, Rashidah |
author_sort |
Abdul Rahim, Rashidah |
title |
Enzymatic Synthesis of Palm Based Fatty Monoethanolamide |
title_short |
Enzymatic Synthesis of Palm Based Fatty Monoethanolamide |
title_full |
Enzymatic Synthesis of Palm Based Fatty Monoethanolamide |
title_fullStr |
Enzymatic Synthesis of Palm Based Fatty Monoethanolamide |
title_full_unstemmed |
Enzymatic Synthesis of Palm Based Fatty Monoethanolamide |
title_sort |
enzymatic synthesis of palm based fatty monoethanolamide |
granting_institution |
Universiti Putra Malaysia |
granting_department |
Faculty of Science and Environmental Studies |
publishDate |
2002 |
url |
http://psasir.upm.edu.my/id/eprint/9523/1/FSAS_2002_53.pdf |
_version_ |
1794018847026577408 |