Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method

Antimony trioxide (Sb2O3) nanoparticles with particle size less than 100 nm, spherical in shape and well distributed were successfully synthesized by chemical reducing method. Antimony trichloride (SbCl3) was reduced by hydrazine in the presence of sodium hydroxide (NaOH) as catalyst in ethylene gly...

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Main Author:	Chin , Hui Shun
Format:	Thesis
Language:	English
Published:	2012
Subjects:	TN1-997 Mining engineering Metallurgy
Online Access:	http://eprints.usm.my/41727/1/CHIN_HUI_SHUN.pdf
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id	my-usm-ep.41727
record_format	uketd_dc
spelling	my-usm-ep.417272019-04-12T05:26:22Z Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method 2012-03 Chin , Hui Shun TN1-997 Mining engineering. Metallurgy Antimony trioxide (Sb2O3) nanoparticles with particle size less than 100 nm, spherical in shape and well distributed were successfully synthesized by chemical reducing method. Antimony trichloride (SbCl3) was reduced by hydrazine in the presence of sodium hydroxide (NaOH) as catalyst in ethylene glycol (EG) at 120 oC for 60 minutes. In order to synthesis Sb2O3 nanoparticles with smaller particle size (2 - 12 nm), spherical in shape and well distribution, effects of hydrazine concentration ([N2H5OH]/[SbCl3] = 0.75, 5, 10, 20 and 30), NaOH concentration ([NaOH]/[SbCl3] = 0, 1, 3 and 5), precursor concentration ([SbCl3]/[N2H5OH] = 0.05, 0.1, 0.15 and 0.2), reaction temperature (60, 90, 120 and 150oC), reaction time (30, 60, 90 and 120 minutes) and boiling temperature (25, 50, 80 and 110oC) were investigated. 2012-03 Thesis http://eprints.usm.my/41727/ http://eprints.usm.my/41727/1/CHIN_HUI_SHUN.pdf application/pdf en public masters Universiti Sains Malaysia Pusat Pengajian Kejuteraan Bahan & Sumber Mineral
institution	Universiti Sains Malaysia
collection	USM Institutional Repository
language	English
topic	TN1-997 Mining engineering Metallurgy
spellingShingle	TN1-997 Mining engineering Metallurgy Chin , Hui Shun Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method
description	Antimony trioxide (Sb2O3) nanoparticles with particle size less than 100 nm, spherical in shape and well distributed were successfully synthesized by chemical reducing method. Antimony trichloride (SbCl3) was reduced by hydrazine in the presence of sodium hydroxide (NaOH) as catalyst in ethylene glycol (EG) at 120 oC for 60 minutes. In order to synthesis Sb2O3 nanoparticles with smaller particle size (2 - 12 nm), spherical in shape and well distribution, effects of hydrazine concentration ([N2H5OH]/[SbCl3] = 0.75, 5, 10, 20 and 30), NaOH concentration ([NaOH]/[SbCl3] = 0, 1, 3 and 5), precursor concentration ([SbCl3]/[N2H5OH] = 0.05, 0.1, 0.15 and 0.2), reaction temperature (60, 90, 120 and 150oC), reaction time (30, 60, 90 and 120 minutes) and boiling temperature (25, 50, 80 and 110oC) were investigated.
format	Thesis
qualification_level	Master's degree
author	Chin , Hui Shun
author_facet	Chin , Hui Shun
author_sort	Chin , Hui Shun
title	Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method
title_short	Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method
title_full	Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method
title_fullStr	Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method
title_full_unstemmed	Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method
title_sort	synthesis and characterization of sb2o3 nanoparticles by chemical reduction method
granting_institution	Universiti Sains Malaysia
granting_department	Pusat Pengajian Kejuteraan Bahan & Sumber Mineral
publishDate	2012
url	http://eprints.usm.my/41727/1/CHIN_HUI_SHUN.pdf
_version_	1747820962482487296

Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method

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