Silica Nanoparticles, Synthesis, Modification And Their Applications In The Fabrication Of Polypyrrolebased Silica Nanocomposites

A modified preparation of silica nanoparticles via sol-gel process is described. The ability to control the particle size and distribution is found to be highly dependent on mixing modes of the reactants and drying techniques. The mixture of tetraethoxysilane (TEOS) and ethanol followed by addition...

Full description

Saved in:
Bibliographic Details
Main Author: Mohammad , Jafarzadeh
Format: Thesis
Language:English
Published: 2010
Subjects:
Online Access:http://eprints.usm.my/42059/1/MOHAMMAD_JAFARZADEH.pdf
Tags: Add Tag
No Tags, Be the first to tag this record!
Description
Summary:A modified preparation of silica nanoparticles via sol-gel process is described. The ability to control the particle size and distribution is found to be highly dependent on mixing modes of the reactants and drying techniques. The mixture of tetraethoxysilane (TEOS) and ethanol followed by addition of water (Mode-A) produce monodispersed powder with an average particle size of 10.6 ± 1.40 nm and a narrow size distribution. The freeze drying technique (FD) further improves the quality of the powder compared to heat drying (HD).