Synthesis And Characterization Of Nanostructured Zinc Oxide (Zno) For Sensor Applications

This project focuses on the development of new approach to grow a variety of high quality ZnO nanostructures without catalyst through a low cost method by wet thermal evaporation for sensor applications. The growth of ZnO nano- and microstructures is by wet oxidation of Zn powder via the vapour–s...

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Main Author: Abdulgafour, Hind I.
Format: Thesis
Language:English
Published: 2013
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Online Access:http://eprints.usm.my/43469/1/Hind%20I.%20Abdulgafour24.pdf
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spelling my-usm-ep.434692019-04-12T05:26:11Z Synthesis And Characterization Of Nanostructured Zinc Oxide (Zno) For Sensor Applications 2013-06 Abdulgafour, Hind I. QC1 Physics (General) This project focuses on the development of new approach to grow a variety of high quality ZnO nanostructures without catalyst through a low cost method by wet thermal evaporation for sensor applications. The growth of ZnO nano- and microstructures is by wet oxidation of Zn powder via the vapour–solid (VS) mechanism. In the first part of this work, the effect of different temperatures on synthesizing high quality ZnO nanostructures on Si/SiO2 substrate was studied. The growth temperatures could be divided into three regions: low (550-650˚C), moderate (700-800˚C), and high (850-900˚C), respectively. The fabrication of high quality ZnO nanostructures for sensor applications was confined in the moderate to high temperature regions. The influence of different durations on the growth of ZnO nanorods was also discussed. Apart from that, a novel fabrication of 3D ZnO microstructures and nanostructures at different temperatures in one step without catalyst was presented. The structural and optical properties as well as the growth mechanisms of various ZnO nanostructures have been investigated and proposed. The best performance device for ZnO tetrapod-like nanorods grown on Si/SiO2 was fabricated to study the effect of thermal annealing temperatures on the electrical properties of Pd/ZnO tetrapod-like nanorods. The enhancement of the photoresponse time of low cost Pd/ZnO tetrapod-like nanorods for ultraviolet (UV) detection was obtained. It was found that the maximum responsivity of the Pd/ZnO metalsemiconductor- metal (MSM) photodetector was 0.106 A/W at 300 nm which corresponds to a quantum efficiency of 43.8% at 5 V applied bias voltage. 2013-06 Thesis http://eprints.usm.my/43469/ http://eprints.usm.my/43469/1/Hind%20I.%20Abdulgafour24.pdf application/pdf en public phd doctoral Universiti Sains Malaysia Pusat Pengajian Sains Fizik
institution Universiti Sains Malaysia
collection USM Institutional Repository
language English
topic QC1 Physics (General)
spellingShingle QC1 Physics (General)
Abdulgafour, Hind I.
Synthesis And Characterization Of Nanostructured Zinc Oxide (Zno) For Sensor Applications
description This project focuses on the development of new approach to grow a variety of high quality ZnO nanostructures without catalyst through a low cost method by wet thermal evaporation for sensor applications. The growth of ZnO nano- and microstructures is by wet oxidation of Zn powder via the vapour–solid (VS) mechanism. In the first part of this work, the effect of different temperatures on synthesizing high quality ZnO nanostructures on Si/SiO2 substrate was studied. The growth temperatures could be divided into three regions: low (550-650˚C), moderate (700-800˚C), and high (850-900˚C), respectively. The fabrication of high quality ZnO nanostructures for sensor applications was confined in the moderate to high temperature regions. The influence of different durations on the growth of ZnO nanorods was also discussed. Apart from that, a novel fabrication of 3D ZnO microstructures and nanostructures at different temperatures in one step without catalyst was presented. The structural and optical properties as well as the growth mechanisms of various ZnO nanostructures have been investigated and proposed. The best performance device for ZnO tetrapod-like nanorods grown on Si/SiO2 was fabricated to study the effect of thermal annealing temperatures on the electrical properties of Pd/ZnO tetrapod-like nanorods. The enhancement of the photoresponse time of low cost Pd/ZnO tetrapod-like nanorods for ultraviolet (UV) detection was obtained. It was found that the maximum responsivity of the Pd/ZnO metalsemiconductor- metal (MSM) photodetector was 0.106 A/W at 300 nm which corresponds to a quantum efficiency of 43.8% at 5 V applied bias voltage.
format Thesis
qualification_name Doctor of Philosophy (PhD.)
qualification_level Doctorate
author Abdulgafour, Hind I.
author_facet Abdulgafour, Hind I.
author_sort Abdulgafour, Hind I.
title Synthesis And Characterization Of Nanostructured Zinc Oxide (Zno) For Sensor Applications
title_short Synthesis And Characterization Of Nanostructured Zinc Oxide (Zno) For Sensor Applications
title_full Synthesis And Characterization Of Nanostructured Zinc Oxide (Zno) For Sensor Applications
title_fullStr Synthesis And Characterization Of Nanostructured Zinc Oxide (Zno) For Sensor Applications
title_full_unstemmed Synthesis And Characterization Of Nanostructured Zinc Oxide (Zno) For Sensor Applications
title_sort synthesis and characterization of nanostructured zinc oxide (zno) for sensor applications
granting_institution Universiti Sains Malaysia
granting_department Pusat Pengajian Sains Fizik
publishDate 2013
url http://eprints.usm.my/43469/1/Hind%20I.%20Abdulgafour24.pdf
_version_ 1747821221255315456