Synthesis, Characterization And Modification Of SAPO-34 Zeolite Membrane For Separation Of CO2 From Binary Gas Mixtures

In the present research, silicoaluminophosphate – thirty four (SAPO-34) zeolite membranes were synthesized on  -alumina disc support using (1) direct insitu crystallization and (2) microwave (MW) heating. MW heating formed thinner SAPO-34 membrane (thickness of ~ 1.6  m) with narrower zeolite crys...

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Main Author:	Chew, Thiam Leng
Format:	Thesis
Language:	English
Published:	2012
Subjects:	TP1-1185 Chemical technology
Online Access:	http://eprints.usm.my/44790/1/CHEW%20THIAM%20LENG.pdf
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spelling	my-usm-ep.447902019-07-01T07:15:01Z Synthesis, Characterization And Modification Of SAPO-34 Zeolite Membrane For Separation Of CO2 From Binary Gas Mixtures 2012-05 Chew, Thiam Leng TP1-1185 Chemical technology In the present research, silicoaluminophosphate – thirty four (SAPO-34) zeolite membranes were synthesized on  -alumina disc support using (1) direct insitu crystallization and (2) microwave (MW) heating. MW heating formed thinner SAPO-34 membrane (thickness of ~ 1.6  m) with narrower zeolite crystal size distribution (~ 0.6  m) in much shortened synthesis time of 2 hours at 200 oC compared to direct in-situ crystallization. The SAPO-34 membranes synthesized using MW heating were modified by ion-exchange process with Mg2+, Ca2+, Sr2+ and Ba2+cations. The membranes were characterized using TEM, XRD, SEM, TGA, EDS, FT-IR and nitrogen adsorption-desorption. 2012-05 Thesis http://eprints.usm.my/44790/ http://eprints.usm.my/44790/1/CHEW%20THIAM%20LENG.pdf application/pdf en public phd doctoral Universiti Sains Malaysia Pusat Pengajian Kejuteraan Kimia
institution	Universiti Sains Malaysia
collection	USM Institutional Repository
language	English
topic	TP1-1185 Chemical technology
spellingShingle	TP1-1185 Chemical technology Chew, Thiam Leng Synthesis, Characterization And Modification Of SAPO-34 Zeolite Membrane For Separation Of CO2 From Binary Gas Mixtures
description	In the present research, silicoaluminophosphate – thirty four (SAPO-34) zeolite membranes were synthesized on  -alumina disc support using (1) direct insitu crystallization and (2) microwave (MW) heating. MW heating formed thinner SAPO-34 membrane (thickness of ~ 1.6  m) with narrower zeolite crystal size distribution (~ 0.6  m) in much shortened synthesis time of 2 hours at 200 oC compared to direct in-situ crystallization. The SAPO-34 membranes synthesized using MW heating were modified by ion-exchange process with Mg2+, Ca2+, Sr2+ and Ba2+cations. The membranes were characterized using TEM, XRD, SEM, TGA, EDS, FT-IR and nitrogen adsorption-desorption.
format	Thesis
qualification_name	Doctor of Philosophy (PhD.)
qualification_level	Doctorate
author	Chew, Thiam Leng
author_facet	Chew, Thiam Leng
author_sort	Chew, Thiam Leng
title	Synthesis, Characterization And Modification Of SAPO-34 Zeolite Membrane For Separation Of CO2 From Binary Gas Mixtures
title_short	Synthesis, Characterization And Modification Of SAPO-34 Zeolite Membrane For Separation Of CO2 From Binary Gas Mixtures
title_full	Synthesis, Characterization And Modification Of SAPO-34 Zeolite Membrane For Separation Of CO2 From Binary Gas Mixtures
title_fullStr	Synthesis, Characterization And Modification Of SAPO-34 Zeolite Membrane For Separation Of CO2 From Binary Gas Mixtures
title_full_unstemmed	Synthesis, Characterization And Modification Of SAPO-34 Zeolite Membrane For Separation Of CO2 From Binary Gas Mixtures
title_sort	synthesis, characterization and modification of sapo-34 zeolite membrane for separation of co2 from binary gas mixtures
granting_institution	Universiti Sains Malaysia
granting_department	Pusat Pengajian Kejuteraan Kimia
publishDate	2012
url	http://eprints.usm.my/44790/1/CHEW%20THIAM%20LENG.pdf
_version_	1747821399533158400

Synthesis, Characterization And Modification Of SAPO-34 Zeolite Membrane For Separation Of CO2 From Binary Gas Mixtures

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