Synthesis And Properties Of Highly Cross-Linked Polysiloxane For LED Encapsulant

The research focuses on the synthesis of two series of polysiloxane. The first series (S1) is hydrosilyl-terminated polydimethylsiloxane (HTP) that was cured with 2,4,6,8-tetramethyl-2,4,6,8-tetravinyl cyclotetrasiloxane (D4V) and second series (S2) is the incorporation of octaphenylcyclotetrasiloxa...

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Main Author: Looi, Yien Tyng
Format: Thesis
Language:English
Published: 2012
Subjects:
Online Access:http://eprints.usm.my/44829/1/LOOI%20YIEN%20TYNG.pdf
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spelling my-usm-ep.448292019-07-03T01:30:51Z Synthesis And Properties Of Highly Cross-Linked Polysiloxane For LED Encapsulant 2012-06 Looi, Yien Tyng TN1-997 Mining engineering. Metallurgy The research focuses on the synthesis of two series of polysiloxane. The first series (S1) is hydrosilyl-terminated polydimethylsiloxane (HTP) that was cured with 2,4,6,8-tetramethyl-2,4,6,8-tetravinyl cyclotetrasiloxane (D4V) and second series (S2) is the incorporation of octaphenylcyclotetrasiloxane (P4) into first series. The polymers of both series underwent thermal curing. UV curing was performed on the first series to improve the curing time as well as comparing their properties. The polysiloxanes product was a water clear gel form. The elastomeric feature of series S1 was dependent on the end-capper concentration, 1,1,3,3- tetramethyldisiloxane while series S2 was dependent on the amount of phenyl group of octaphenylcyclotetrasiloxane (P4) employed during its synthesis. FTIR and NMR was used to confirm the functional group of HTP and completion of the hydrosilylation reaction. 2012-06 Thesis http://eprints.usm.my/44829/ http://eprints.usm.my/44829/1/LOOI%20YIEN%20TYNG.pdf application/pdf en public masters Universiti Sains Malaysia Pusat Pengajian Kejuteraan Bahan & Sumber Mineral
institution Universiti Sains Malaysia
collection USM Institutional Repository
language English
topic TN1-997 Mining engineering
Metallurgy
spellingShingle TN1-997 Mining engineering
Metallurgy
Looi, Yien Tyng
Synthesis And Properties Of Highly Cross-Linked Polysiloxane For LED Encapsulant
description The research focuses on the synthesis of two series of polysiloxane. The first series (S1) is hydrosilyl-terminated polydimethylsiloxane (HTP) that was cured with 2,4,6,8-tetramethyl-2,4,6,8-tetravinyl cyclotetrasiloxane (D4V) and second series (S2) is the incorporation of octaphenylcyclotetrasiloxane (P4) into first series. The polymers of both series underwent thermal curing. UV curing was performed on the first series to improve the curing time as well as comparing their properties. The polysiloxanes product was a water clear gel form. The elastomeric feature of series S1 was dependent on the end-capper concentration, 1,1,3,3- tetramethyldisiloxane while series S2 was dependent on the amount of phenyl group of octaphenylcyclotetrasiloxane (P4) employed during its synthesis. FTIR and NMR was used to confirm the functional group of HTP and completion of the hydrosilylation reaction.
format Thesis
qualification_level Master's degree
author Looi, Yien Tyng
author_facet Looi, Yien Tyng
author_sort Looi, Yien Tyng
title Synthesis And Properties Of Highly Cross-Linked Polysiloxane For LED Encapsulant
title_short Synthesis And Properties Of Highly Cross-Linked Polysiloxane For LED Encapsulant
title_full Synthesis And Properties Of Highly Cross-Linked Polysiloxane For LED Encapsulant
title_fullStr Synthesis And Properties Of Highly Cross-Linked Polysiloxane For LED Encapsulant
title_full_unstemmed Synthesis And Properties Of Highly Cross-Linked Polysiloxane For LED Encapsulant
title_sort synthesis and properties of highly cross-linked polysiloxane for led encapsulant
granting_institution Universiti Sains Malaysia
granting_department Pusat Pengajian Kejuteraan Bahan & Sumber Mineral
publishDate 2012
url http://eprints.usm.my/44829/1/LOOI%20YIEN%20TYNG.pdf
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