Characterization, Thermal And Mechanical Properties Of Tropical Plant Fibres

The work deals with systematic evaluation of chemical, morphological, anatomical, thermal and mechanical properties of tropical plant fibres. The TAPPI test standard and Fourier transform infrared (FT-IR) spectroscopy were used to study the chemical composition and spectroscopic properties of plant...

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Main Author: Mohamed, Fibres Siti Alwani
Format: Thesis
Language:English
Published: 2013
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Online Access:http://eprints.usm.my/46240/1/Siti%20Alwani%20Mohamed24.pdf
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spelling my-usm-ep.462402020-02-17T03:33:01Z Characterization, Thermal And Mechanical Properties Of Tropical Plant Fibres 2013-12 Mohamed, Fibres Siti Alwani T11.95-12.5 Industrial directories The work deals with systematic evaluation of chemical, morphological, anatomical, thermal and mechanical properties of tropical plant fibres. The TAPPI test standard and Fourier transform infrared (FT-IR) spectroscopy were used to study the chemical composition and spectroscopic properties of plant fibre. The crystallinity was determined using X-ray diffraction (XRD). Light microscopy (LM) and transmission electron microscopy (TEM) were used to observe the morphology and cell wall structure of the fibre. Lignin distribution across cell wall layers was analyzed using scanning electron microscopy coupled with x-ray energy dispersive (SEM-EDX) and Raman spectroscopy. In addition, thermogravimetry analysis (TGA) was used to investigate thermal stability of the fibres. Meanwhile, miniature tensile tester also was used to measure the mechanical properties of fibres. Four different types of plant fibre were chosen which include coconut (COIR), banana pseudo-stem (BPS), pineapple leaf (PALF) and sugarcane bagasse (SCB) fibres for the study. Moisture content in all types of plant fibre studied was in the range between 6-9%. Cellulose content was highest in PALF (70%) while lignin was highest in COIR (28%). Meanwhile, SCB consists of the highest hemicelluloses content (10%) compared to other fibres and ash content was the highest in BPS (2.2%). Crystallinity was calculated by to peak height and deconvulated peak method. However, the results were completely different for these two methods. COIR showed the highest crystallinity (52.0%) by peak height method, whereas it was the highest in PALF (68.3%) when calculated by peak deconvulated method. 2013-12 Thesis http://eprints.usm.my/46240/ http://eprints.usm.my/46240/1/Siti%20Alwani%20Mohamed24.pdf application/pdf en public phd doctoral Universiti Sains Malaysia Pusat Pengajian Teknologi Industri
institution Universiti Sains Malaysia
collection USM Institutional Repository
language English
topic T11.95-12.5 Industrial directories
spellingShingle T11.95-12.5 Industrial directories
Mohamed, Fibres Siti Alwani
Characterization, Thermal And Mechanical Properties Of Tropical Plant Fibres
description The work deals with systematic evaluation of chemical, morphological, anatomical, thermal and mechanical properties of tropical plant fibres. The TAPPI test standard and Fourier transform infrared (FT-IR) spectroscopy were used to study the chemical composition and spectroscopic properties of plant fibre. The crystallinity was determined using X-ray diffraction (XRD). Light microscopy (LM) and transmission electron microscopy (TEM) were used to observe the morphology and cell wall structure of the fibre. Lignin distribution across cell wall layers was analyzed using scanning electron microscopy coupled with x-ray energy dispersive (SEM-EDX) and Raman spectroscopy. In addition, thermogravimetry analysis (TGA) was used to investigate thermal stability of the fibres. Meanwhile, miniature tensile tester also was used to measure the mechanical properties of fibres. Four different types of plant fibre were chosen which include coconut (COIR), banana pseudo-stem (BPS), pineapple leaf (PALF) and sugarcane bagasse (SCB) fibres for the study. Moisture content in all types of plant fibre studied was in the range between 6-9%. Cellulose content was highest in PALF (70%) while lignin was highest in COIR (28%). Meanwhile, SCB consists of the highest hemicelluloses content (10%) compared to other fibres and ash content was the highest in BPS (2.2%). Crystallinity was calculated by to peak height and deconvulated peak method. However, the results were completely different for these two methods. COIR showed the highest crystallinity (52.0%) by peak height method, whereas it was the highest in PALF (68.3%) when calculated by peak deconvulated method.
format Thesis
qualification_name Doctor of Philosophy (PhD.)
qualification_level Doctorate
author Mohamed, Fibres Siti Alwani
author_facet Mohamed, Fibres Siti Alwani
author_sort Mohamed, Fibres Siti Alwani
title Characterization, Thermal And Mechanical Properties Of Tropical Plant Fibres
title_short Characterization, Thermal And Mechanical Properties Of Tropical Plant Fibres
title_full Characterization, Thermal And Mechanical Properties Of Tropical Plant Fibres
title_fullStr Characterization, Thermal And Mechanical Properties Of Tropical Plant Fibres
title_full_unstemmed Characterization, Thermal And Mechanical Properties Of Tropical Plant Fibres
title_sort characterization, thermal and mechanical properties of tropical plant fibres
granting_institution Universiti Sains Malaysia
granting_department Pusat Pengajian Teknologi Industri
publishDate 2013
url http://eprints.usm.my/46240/1/Siti%20Alwani%20Mohamed24.pdf
_version_ 1747821634836758528