Physicochemical And Emulsifying Properties Of Pre-Treated Octenyl Succinic Anhydride (Osa) Sago Starch In Emulsion

Sago starch is abundant in Malaysia and it has the potential to be used as an emulsifier. However, native starch is generally hydrophilic and there is a need to increase its hydrophobicity by modification in order to increase its ability to stabilize emulsion. Therefore, this research was designed t...

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Main Author: Saw, Sue San
Format: Thesis
Language:English
Published: 2021
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Online Access:http://eprints.usm.my/52562/1/SAW%20SUE%20SAN.pdf
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spelling my-usm-ep.525622022-05-23T07:20:00Z Physicochemical And Emulsifying Properties Of Pre-Treated Octenyl Succinic Anhydride (Osa) Sago Starch In Emulsion 2021-03 Saw, Sue San T1-995 Technology(General) T175-178 Industrial research. Research and development Sago starch is abundant in Malaysia and it has the potential to be used as an emulsifier. However, native starch is generally hydrophilic and there is a need to increase its hydrophobicity by modification in order to increase its ability to stabilize emulsion. Therefore, this research was designed to increase the hydrophobicity as well as effectiveness of sago starch as an emulsifier. In this study, sago starch was pre-treated with heat moisture treatment (HMT) (single pre-treatment), STARGEN enzyme (single pre-treatment), and heat moisture treatment followed by STARGEN enzyme (dual pre-treatment) prior to octenyl succinic anhydride (OSA) modification. Enzyme-treated OSA (EN OSA) showed the highest degree of substitution (DS) (0.0152) followed by heat moisture-enzyme-treated OSA (HMT EN OSA) (0.0119) and heat moisture-treated OSA (HMT OSA) (0.0105). SEM micrograph revealed rough surface with their edges lose some definition for all OSA modified starches. Among all samples, EN OSA showed the smallest particle size, where the particle size of EN OSA had reduced from 31 μm to 28 μm. The ability of all pre-treated OSA sago starches to stabilize emulsion was then investigated. Compared to other starches, EN OSA had significantly highest emulsifying activity and produced a thick viscous emulsion layer after emulsification. After 56th days (8th week) of storage at room temperature, EN OSA showed the highest stability by exhibiting the highest emulsion index which is between 0.37 (starch concentration 200 mg / mL) to 0.56 (starch concentration 500 mg/mL). 2021-03 Thesis http://eprints.usm.my/52562/ http://eprints.usm.my/52562/1/SAW%20SUE%20SAN.pdf application/pdf en public masters Perpustakaan Hamzah Sendut Pusat Pengajian Teknologi Industri
institution Universiti Sains Malaysia
collection USM Institutional Repository
language English
topic T1-995 Technology(General)
T1-995 Technology(General)
spellingShingle T1-995 Technology(General)
T1-995 Technology(General)
Saw, Sue San
Physicochemical And Emulsifying Properties Of Pre-Treated Octenyl Succinic Anhydride (Osa) Sago Starch In Emulsion
description Sago starch is abundant in Malaysia and it has the potential to be used as an emulsifier. However, native starch is generally hydrophilic and there is a need to increase its hydrophobicity by modification in order to increase its ability to stabilize emulsion. Therefore, this research was designed to increase the hydrophobicity as well as effectiveness of sago starch as an emulsifier. In this study, sago starch was pre-treated with heat moisture treatment (HMT) (single pre-treatment), STARGEN enzyme (single pre-treatment), and heat moisture treatment followed by STARGEN enzyme (dual pre-treatment) prior to octenyl succinic anhydride (OSA) modification. Enzyme-treated OSA (EN OSA) showed the highest degree of substitution (DS) (0.0152) followed by heat moisture-enzyme-treated OSA (HMT EN OSA) (0.0119) and heat moisture-treated OSA (HMT OSA) (0.0105). SEM micrograph revealed rough surface with their edges lose some definition for all OSA modified starches. Among all samples, EN OSA showed the smallest particle size, where the particle size of EN OSA had reduced from 31 μm to 28 μm. The ability of all pre-treated OSA sago starches to stabilize emulsion was then investigated. Compared to other starches, EN OSA had significantly highest emulsifying activity and produced a thick viscous emulsion layer after emulsification. After 56th days (8th week) of storage at room temperature, EN OSA showed the highest stability by exhibiting the highest emulsion index which is between 0.37 (starch concentration 200 mg / mL) to 0.56 (starch concentration 500 mg/mL).
format Thesis
qualification_level Master's degree
author Saw, Sue San
author_facet Saw, Sue San
author_sort Saw, Sue San
title Physicochemical And Emulsifying Properties Of Pre-Treated Octenyl Succinic Anhydride (Osa) Sago Starch In Emulsion
title_short Physicochemical And Emulsifying Properties Of Pre-Treated Octenyl Succinic Anhydride (Osa) Sago Starch In Emulsion
title_full Physicochemical And Emulsifying Properties Of Pre-Treated Octenyl Succinic Anhydride (Osa) Sago Starch In Emulsion
title_fullStr Physicochemical And Emulsifying Properties Of Pre-Treated Octenyl Succinic Anhydride (Osa) Sago Starch In Emulsion
title_full_unstemmed Physicochemical And Emulsifying Properties Of Pre-Treated Octenyl Succinic Anhydride (Osa) Sago Starch In Emulsion
title_sort physicochemical and emulsifying properties of pre-treated octenyl succinic anhydride (osa) sago starch in emulsion
granting_institution Perpustakaan Hamzah Sendut
granting_department Pusat Pengajian Teknologi Industri
publishDate 2021
url http://eprints.usm.my/52562/1/SAW%20SUE%20SAN.pdf
_version_ 1747822191749103616