Synthesis And Characterization Of Mg-Substituted Biphasic Calcium Phosphate

Sample without magnesium (Mg) and Mg-substituted biphasic calcium phosphate (BCP) were synthesized through precipitation method at room temperature. The substitution of Mg in BCP were considered due to Mg being one of the main element found in human bones. Hence, this study emphasize more on the eff...

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Main Author:	Mohd. Moslim, Nur Atiqqah
Format:	Thesis
Language:	English
Published:	2019
Subjects:	T Technology
Online Access:	http://eprints.usm.my/55397/1/Synthesis%20And%20Characterization%20Of%20Mg-Substituted%20Biphasic%20Calcium%20Phosphate_Nur%20Atiqqah%20Mohd.%20Moslim.pdf
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spelling	my-usm-ep.553972022-10-20T06:19:36Z Synthesis And Characterization Of Mg-Substituted Biphasic Calcium Phosphate 2019-08-01 Mohd. Moslim, Nur Atiqqah T Technology TN Mining Engineering. Metallurgy Sample without magnesium (Mg) and Mg-substituted biphasic calcium phosphate (BCP) were synthesized through precipitation method at room temperature. The substitution of Mg in BCP were considered due to Mg being one of the main element found in human bones. Hence, this study emphasize more on the effect of Mg substitutions towards phase formations with regards to three parameters which are the concentration of Mg ions, the molar ratio between precursors, and the calcination temperature. The as-synthesized sample without Mg BCP shows the formation of monetite and hydroxyapatite (HA) phase while the Mg-substituted BCP show only HA phase exist. As for the calcined BCP powders at 600 °C, both without Mg and Mg-substituted samples shows biphasic formation of HA and beta-tricalcium phosphate (β-TCP). BCP with the highest Mg ions concentration exhibit the highest β-TCP phase formation (75.3 wt %) while the without substituted BCP sample has the lowest β-TCP formation (20.5 wt %). It shows an increasing trend of β-TCP phase with the increase of Mg concentration. The different molar ratio between precursors does not give subtle effect on the phase formations as compared to the effect of Mg concentrations. BCP powders calcined at lower temperature of 500 °C shows less formation of β-TCP phase when compared to sample calcined at 600 °C. This results proved that the phase transition of BCP from HA to β-TCP were enhanced when subjected to high calcination temperature. 2019-08 Thesis http://eprints.usm.my/55397/ http://eprints.usm.my/55397/1/Synthesis%20And%20Characterization%20Of%20Mg-Substituted%20Biphasic%20Calcium%20Phosphate_Nur%20Atiqqah%20Mohd.%20Moslim.pdf application/pdf en public masters Universiti Sains Malaysia Pusat Pengajian Kejuruteraan Bahan dan Sumber Mineral
institution	Universiti Sains Malaysia
collection	USM Institutional Repository
language	English
topic	T Technology T Technology
spellingShingle	T Technology T Technology Mohd. Moslim, Nur Atiqqah Synthesis And Characterization Of Mg-Substituted Biphasic Calcium Phosphate
description	Sample without magnesium (Mg) and Mg-substituted biphasic calcium phosphate (BCP) were synthesized through precipitation method at room temperature. The substitution of Mg in BCP were considered due to Mg being one of the main element found in human bones. Hence, this study emphasize more on the effect of Mg substitutions towards phase formations with regards to three parameters which are the concentration of Mg ions, the molar ratio between precursors, and the calcination temperature. The as-synthesized sample without Mg BCP shows the formation of monetite and hydroxyapatite (HA) phase while the Mg-substituted BCP show only HA phase exist. As for the calcined BCP powders at 600 °C, both without Mg and Mg-substituted samples shows biphasic formation of HA and beta-tricalcium phosphate (β-TCP). BCP with the highest Mg ions concentration exhibit the highest β-TCP phase formation (75.3 wt %) while the without substituted BCP sample has the lowest β-TCP formation (20.5 wt %). It shows an increasing trend of β-TCP phase with the increase of Mg concentration. The different molar ratio between precursors does not give subtle effect on the phase formations as compared to the effect of Mg concentrations. BCP powders calcined at lower temperature of 500 °C shows less formation of β-TCP phase when compared to sample calcined at 600 °C. This results proved that the phase transition of BCP from HA to β-TCP were enhanced when subjected to high calcination temperature.
format	Thesis
qualification_level	Master's degree
author	Mohd. Moslim, Nur Atiqqah
author_facet	Mohd. Moslim, Nur Atiqqah
author_sort	Mohd. Moslim, Nur Atiqqah
title	Synthesis And Characterization Of Mg-Substituted Biphasic Calcium Phosphate
title_short	Synthesis And Characterization Of Mg-Substituted Biphasic Calcium Phosphate
title_full	Synthesis And Characterization Of Mg-Substituted Biphasic Calcium Phosphate
title_fullStr	Synthesis And Characterization Of Mg-Substituted Biphasic Calcium Phosphate
title_full_unstemmed	Synthesis And Characterization Of Mg-Substituted Biphasic Calcium Phosphate
title_sort	synthesis and characterization of mg-substituted biphasic calcium phosphate
granting_institution	Universiti Sains Malaysia
granting_department	Pusat Pengajian Kejuruteraan Bahan dan Sumber Mineral
publishDate	2019
url	http://eprints.usm.my/55397/1/Synthesis%20And%20Characterization%20Of%20Mg-Substituted%20Biphasic%20Calcium%20Phosphate_Nur%20Atiqqah%20Mohd.%20Moslim.pdf
_version_	1747822322037817344

Synthesis And Characterization Of Mg-Substituted Biphasic Calcium Phosphate

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