Synthesis And Characterisation Of Colloidal Alpo-S Nanocrystals Templated By L-Ethyl-2,3- Dimetiiylimidazolium Hydroxide
Colloidal stable nanosized AIPO-S crystals were synthesised via hydrothermal method using a new template, l-ethyl-2,3-dimethylimidazolium hydroxide, [edmim]OH. The syntheses were carried out under various synthesis conditions such as heating time, heating temperature and molar composition of pre...
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my-usm-ep.608512024-07-18T02:13:53Z Synthesis And Characterisation Of Colloidal Alpo-S Nanocrystals Templated By L-Ethyl-2,3- Dimetiiylimidazolium Hydroxide 2015-01 Ng Tat Lun, Darren T1-995 Technology(General) Colloidal stable nanosized AIPO-S crystals were synthesised via hydrothermal method using a new template, l-ethyl-2,3-dimethylimidazolium hydroxide, [edmim]OH. The syntheses were carried out under various synthesis conditions such as heating time, heating temperature and molar composition of precursor gels to investigate the effects of the conditions on the crystallisation of AIPO-S. The new template, [edmim]OH, had produced colloidally stable AIPO-S nanocrystals with the size in the range of SO-800 nm with low agglomeration and defined shape. Additionally, this study also applied a facile and fast synthesis method whereby the precursor gels were heated with microwave radiation rather than the conventional heating in an oven. This synthesis method allowed AIPO-S nanocrystals to be obtained within several minutes compared to the conventional hydrothermal heating which required several hours for complete crystallisation. Interestingly, the nanocrystals obtained via microwave heating were of smaller sizes due to fast nucleation. The AIPO-S nanocrystals obtained in this study exhibited hexagonal frustum feature with low agglomeration. 2015-01 Thesis http://eprints.usm.my/60851/ http://eprints.usm.my/60851/1/24%20Pages%20from%2000001785176.pdf application/pdf en public masters Perpustakaan Hamzah Sendut Pusat Pengajian Teknologi Industri |
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Universiti Sains Malaysia |
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USM Institutional Repository |
| language |
English |
| topic |
T1-995 Technology(General) |
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T1-995 Technology(General) Ng Tat Lun, Darren Synthesis And Characterisation Of Colloidal Alpo-S Nanocrystals Templated By L-Ethyl-2,3- Dimetiiylimidazolium Hydroxide |
| description |
Colloidal stable nanosized AIPO-S crystals were synthesised via
hydrothermal method using a new template, l-ethyl-2,3-dimethylimidazolium
hydroxide, [edmim]OH. The syntheses were carried out under various synthesis
conditions such as heating time, heating temperature and molar composition of
precursor gels to investigate the effects of the conditions on the crystallisation of
AIPO-S. The new template, [edmim]OH, had produced colloidally stable AIPO-S
nanocrystals with the size in the range of SO-800 nm with low agglomeration and
defined shape. Additionally, this study also applied a facile and fast synthesis method
whereby the precursor gels were heated with microwave radiation rather than the
conventional heating in an oven. This synthesis method allowed AIPO-S nanocrystals
to be obtained within several minutes compared to the conventional hydrothermal
heating which required several hours for complete crystallisation. Interestingly, the
nanocrystals obtained via microwave heating were of smaller sizes due to fast
nucleation. The AIPO-S nanocrystals obtained in this study exhibited hexagonal
frustum feature with low agglomeration. |
| format |
Thesis |
| qualification_level |
Master's degree |
| author |
Ng Tat Lun, Darren |
| author_facet |
Ng Tat Lun, Darren |
| author_sort |
Ng Tat Lun, Darren |
| title |
Synthesis And Characterisation Of Colloidal Alpo-S Nanocrystals Templated By L-Ethyl-2,3- Dimetiiylimidazolium Hydroxide |
| title_short |
Synthesis And Characterisation Of Colloidal Alpo-S Nanocrystals Templated By L-Ethyl-2,3- Dimetiiylimidazolium Hydroxide |
| title_full |
Synthesis And Characterisation Of Colloidal Alpo-S Nanocrystals Templated By L-Ethyl-2,3- Dimetiiylimidazolium Hydroxide |
| title_fullStr |
Synthesis And Characterisation Of Colloidal Alpo-S Nanocrystals Templated By L-Ethyl-2,3- Dimetiiylimidazolium Hydroxide |
| title_full_unstemmed |
Synthesis And Characterisation Of Colloidal Alpo-S Nanocrystals Templated By L-Ethyl-2,3- Dimetiiylimidazolium Hydroxide |
| title_sort |
synthesis and characterisation of colloidal alpo-s nanocrystals templated by l-ethyl-2,3- dimetiiylimidazolium hydroxide |
| granting_institution |
Perpustakaan Hamzah Sendut |
| granting_department |
Pusat Pengajian Teknologi Industri |
| publishDate |
2015 |
| url |
http://eprints.usm.my/60851/1/24%20Pages%20from%2000001785176.pdf |
| _version_ |
1804889007781314560 |