Fabrication and characterisation of Cobalt Chromium Molybdenum (CoCrMo) foams using slurry method

Cobalt Chromium Molybdenum (CoCrMo) is a metal foams that are widely used in the biomedical field of orthopedic applications. This research is intended to produce CoCrMo foam by using slurry method and to perform optimization on processing parameters slurry method in CoCrMo foam preparation by the o...

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Main Author: Ab Manaf, Nur Suliani
Format: Thesis
Language:English
English
English
Published: 2018
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spelling my-uthm-ep.2212021-07-13T01:22:17Z Fabrication and characterisation of Cobalt Chromium Molybdenum (CoCrMo) foams using slurry method 2018-07 Ab Manaf, Nur Suliani QD146-197 Inorganic chemistry Cobalt Chromium Molybdenum (CoCrMo) is a metal foams that are widely used in the biomedical field of orthopedic applications. This research is intended to produce CoCrMo foam by using slurry method and to perform optimization on processing parameters slurry method in CoCrMo foam preparation by the orthogonal array L9 method. The slurry of CoCrMo is prepared by the mixing the binder materials and distilled water for an hour. Followed by mixing and stirring the CoCrMo powder for another 1 hour until it becomes slurries. Polyurethane (PU) foam is then impregnated into the slurry and dried at 40°C for a day in the oven. It was found that the possible composition were 60wt%, 65wt% and 70wt% for CoCrMo. This was followed by the appropriate sintering temperature results which were 1000°C, 1100°C and 1200°C with heating rate of 1.5°C/min, 1.0°C/min and 0.5°C/min. Moreover, for the soaking time factor, the relevant durations were 60, 90 and 120 minutes. The parameter that influence in the result was the composition that were in porosity and bulk density analysis. The optimum value of 54.42% was obtained for porosity was the composition at 60wt% CoCrMo, sintering temperature of 1100°C, heating rate of 1.5°C/min and soaking time of 60 minutes. In addition, the significant factors that influence the bulk density analysis of CoCrMo foam were the composition factor. The optimum sintering condition which resulted in bulk density analysis of 2.23g/cm3 was found to be a composition of CoCrMo at 60wt%, sintering temperature of 1000°C, heating rate of 1.5 °C/min and soaking time of 60 minutes. The present work shows that the optimisation of the sintering parameters has improved the physical properties of both the CoCrMo foams. 2018-07 Thesis http://eprints.uthm.edu.my/221/ http://eprints.uthm.edu.my/221/1/24p%20NUR%20SULIANI%20BINTI%20AB%20MANAF.pdf text en public http://eprints.uthm.edu.my/221/2/NUR%20SULIANI%20BINTI%20AB%20MANAF%20COPYRIGHT%20DECLARATION.pdf text en staffonly http://eprints.uthm.edu.my/221/3/NUR%20SULIANI%20BINTI%20AB%20MANAF%20WATERMARK.pdf text en validuser mphil masters Universiti Tun Hussein Onn Malaysia Faculty of Mechanical and Manufacturing Engineering
institution Universiti Tun Hussein Onn Malaysia
collection UTHM Institutional Repository
language English
English
English
topic QD146-197 Inorganic chemistry
spellingShingle QD146-197 Inorganic chemistry
Ab Manaf, Nur Suliani
Fabrication and characterisation of Cobalt Chromium Molybdenum (CoCrMo) foams using slurry method
description Cobalt Chromium Molybdenum (CoCrMo) is a metal foams that are widely used in the biomedical field of orthopedic applications. This research is intended to produce CoCrMo foam by using slurry method and to perform optimization on processing parameters slurry method in CoCrMo foam preparation by the orthogonal array L9 method. The slurry of CoCrMo is prepared by the mixing the binder materials and distilled water for an hour. Followed by mixing and stirring the CoCrMo powder for another 1 hour until it becomes slurries. Polyurethane (PU) foam is then impregnated into the slurry and dried at 40°C for a day in the oven. It was found that the possible composition were 60wt%, 65wt% and 70wt% for CoCrMo. This was followed by the appropriate sintering temperature results which were 1000°C, 1100°C and 1200°C with heating rate of 1.5°C/min, 1.0°C/min and 0.5°C/min. Moreover, for the soaking time factor, the relevant durations were 60, 90 and 120 minutes. The parameter that influence in the result was the composition that were in porosity and bulk density analysis. The optimum value of 54.42% was obtained for porosity was the composition at 60wt% CoCrMo, sintering temperature of 1100°C, heating rate of 1.5°C/min and soaking time of 60 minutes. In addition, the significant factors that influence the bulk density analysis of CoCrMo foam were the composition factor. The optimum sintering condition which resulted in bulk density analysis of 2.23g/cm3 was found to be a composition of CoCrMo at 60wt%, sintering temperature of 1000°C, heating rate of 1.5 °C/min and soaking time of 60 minutes. The present work shows that the optimisation of the sintering parameters has improved the physical properties of both the CoCrMo foams.
format Thesis
qualification_name Master of Philosophy (M.Phil.)
qualification_level Master's degree
author Ab Manaf, Nur Suliani
author_facet Ab Manaf, Nur Suliani
author_sort Ab Manaf, Nur Suliani
title Fabrication and characterisation of Cobalt Chromium Molybdenum (CoCrMo) foams using slurry method
title_short Fabrication and characterisation of Cobalt Chromium Molybdenum (CoCrMo) foams using slurry method
title_full Fabrication and characterisation of Cobalt Chromium Molybdenum (CoCrMo) foams using slurry method
title_fullStr Fabrication and characterisation of Cobalt Chromium Molybdenum (CoCrMo) foams using slurry method
title_full_unstemmed Fabrication and characterisation of Cobalt Chromium Molybdenum (CoCrMo) foams using slurry method
title_sort fabrication and characterisation of cobalt chromium molybdenum (cocrmo) foams using slurry method
granting_institution Universiti Tun Hussein Onn Malaysia
granting_department Faculty of Mechanical and Manufacturing Engineering
publishDate 2018
url http://eprints.uthm.edu.my/221/1/24p%20NUR%20SULIANI%20BINTI%20AB%20MANAF.pdf
http://eprints.uthm.edu.my/221/2/NUR%20SULIANI%20BINTI%20AB%20MANAF%20COPYRIGHT%20DECLARATION.pdf
http://eprints.uthm.edu.my/221/3/NUR%20SULIANI%20BINTI%20AB%20MANAF%20WATERMARK.pdf
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