Production of biodiesel from waste cooking oil using ultrasonic tubular reactor

The aim of study is to produce the synthesis of biodiesel from waste cooking oil (WCO) using ultrasonic tubular reactor at laboratory scale. The experiment was used to determine the effect of ester contents by reaction time, molar ratio of WCO to Methanol (MeOH), amount of catalyst, frequency...

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Main Author:	Agustian, Egi
Format:	Thesis
Language:	English English English
Published:	2012
Subjects:	TP Chemical technology TP315-360 Fuel
Online Access:	http://eprints.uthm.edu.my/2261/1/24p%20EGI%20AGUSTIAN.pdf http://eprints.uthm.edu.my/2261/2/EGI%20AGUSTIAN%20COPYRIGHT%20DECLARATION.pdf http://eprints.uthm.edu.my/2261/3/EGI%20AGUSTIAN%20WATERMARK.pdf
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id	my-uthm-ep.2261
record_format	uketd_dc
spelling	my-uthm-ep.22612021-10-31T04:50:57Z Production of biodiesel from waste cooking oil using ultrasonic tubular reactor 2012-07 Agustian, Egi TP Chemical technology TP315-360 Fuel The aim of study is to produce the synthesis of biodiesel from waste cooking oil (WCO) using ultrasonic tubular reactor at laboratory scale. The experiment was used to determine the effect of ester contents by reaction time, molar ratio of WCO to Methanol (MeOH), amount of catalyst, frequency of ultrasonic and ultrasonic output power using ultrasonic tubular reactor. Based on the optimum process by ultrasonic tubular reactor, a comparisons study of three different processes (ultrasonic tubular reactor, conventional ultrasonic cleaner and mechanical stirring) were also investigated. The optimum results of biodiesel process using ultrasonic tubular reactor are the reaction time of 5 minute, sodium hydroxide (NaOH) catalyst 1%wt of WCO, molar ratio WCO to MeOH of 1:6, frequency ultrasonic of 20 KHz and ultrasonic output power of 650 Watt. The reaction time was reduced to 12-24 times (minute) compare to mechanical stirring and the ester contents was obtained at 96.54%wt. The ternary phase diagram ultrasonic tubular reactor was to find out the liquid liquid-equilibrium base on WCO- Fatty Acid Methyl Esters (FAME) -MeOH. The results show that by increasing the residence time of the whole reactant system within the two-phase zone is good for the reaction transesterification on ultrasonic tubular reactor. The semi continuous ultrasonic tubular reactor for biodiesel process of WCO gave conversion of WCO to FAME of 98%wt with flow rate of 5.56 ml/s. Meanwhile, the pilot plan of biodiesel facilities using mechanical stirring method (capacity of 100 kg WCO/batch) was designed and the transfer knowledge about biodiesel process was a success between the university with industry in Batu Pahat. 2012-07 Thesis http://eprints.uthm.edu.my/2261/ http://eprints.uthm.edu.my/2261/1/24p%20EGI%20AGUSTIAN.pdf text en public http://eprints.uthm.edu.my/2261/2/EGI%20AGUSTIAN%20COPYRIGHT%20DECLARATION.pdf text en staffonly http://eprints.uthm.edu.my/2261/3/EGI%20AGUSTIAN%20WATERMARK.pdf text en validuser mphil masters Universiti Tun Hussein Onn Malaysia Fakulti Kejuruteraan Mekanikal dan Pembuatan
institution	Universiti Tun Hussein Onn Malaysia
collection	UTHM Institutional Repository
language	English English English
topic	TP Chemical technology TP315-360 Fuel
spellingShingle	TP Chemical technology TP315-360 Fuel Agustian, Egi Production of biodiesel from waste cooking oil using ultrasonic tubular reactor
description	The aim of study is to produce the synthesis of biodiesel from waste cooking oil (WCO) using ultrasonic tubular reactor at laboratory scale. The experiment was used to determine the effect of ester contents by reaction time, molar ratio of WCO to Methanol (MeOH), amount of catalyst, frequency of ultrasonic and ultrasonic output power using ultrasonic tubular reactor. Based on the optimum process by ultrasonic tubular reactor, a comparisons study of three different processes (ultrasonic tubular reactor, conventional ultrasonic cleaner and mechanical stirring) were also investigated. The optimum results of biodiesel process using ultrasonic tubular reactor are the reaction time of 5 minute, sodium hydroxide (NaOH) catalyst 1%wt of WCO, molar ratio WCO to MeOH of 1:6, frequency ultrasonic of 20 KHz and ultrasonic output power of 650 Watt. The reaction time was reduced to 12-24 times (minute) compare to mechanical stirring and the ester contents was obtained at 96.54%wt. The ternary phase diagram ultrasonic tubular reactor was to find out the liquid liquid-equilibrium base on WCO- Fatty Acid Methyl Esters (FAME) -MeOH. The results show that by increasing the residence time of the whole reactant system within the two-phase zone is good for the reaction transesterification on ultrasonic tubular reactor. The semi continuous ultrasonic tubular reactor for biodiesel process of WCO gave conversion of WCO to FAME of 98%wt with flow rate of 5.56 ml/s. Meanwhile, the pilot plan of biodiesel facilities using mechanical stirring method (capacity of 100 kg WCO/batch) was designed and the transfer knowledge about biodiesel process was a success between the university with industry in Batu Pahat.
format	Thesis
qualification_name	Master of Philosophy (M.Phil.)
qualification_level	Master's degree
author	Agustian, Egi
author_facet	Agustian, Egi
author_sort	Agustian, Egi
title	Production of biodiesel from waste cooking oil using ultrasonic tubular reactor
title_short	Production of biodiesel from waste cooking oil using ultrasonic tubular reactor
title_full	Production of biodiesel from waste cooking oil using ultrasonic tubular reactor
title_fullStr	Production of biodiesel from waste cooking oil using ultrasonic tubular reactor
title_full_unstemmed	Production of biodiesel from waste cooking oil using ultrasonic tubular reactor
title_sort	production of biodiesel from waste cooking oil using ultrasonic tubular reactor
granting_institution	Universiti Tun Hussein Onn Malaysia
granting_department	Fakulti Kejuruteraan Mekanikal dan Pembuatan
publishDate	2012
url	http://eprints.uthm.edu.my/2261/1/24p%20EGI%20AGUSTIAN.pdf http://eprints.uthm.edu.my/2261/2/EGI%20AGUSTIAN%20COPYRIGHT%20DECLARATION.pdf http://eprints.uthm.edu.my/2261/3/EGI%20AGUSTIAN%20WATERMARK.pdf
_version_	1747830930676908032

Production of biodiesel from waste cooking oil using ultrasonic tubular reactor

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