Controlled release formulation of paddy pesticides intercalated layered metal hydroxide via polysaccharide encapsulation

This research aimed to synthesis intercalated nanocomposites of paddy pesticides forcontrolled release formulation (CRF), namely zinc/aluminiumlayered doublehydroxidequinclorac (Zn/AlLDHQC), zinc hydroxide nitratesodiumdodecylsulphatebispyribac (ZHNSDSBP) and zinc hydroxide nitratesodiumdodecylsulph...

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Main Author:	Sharifah Norain Mohd Sharif
Format:	thesis
Language:	eng
Published:	2019
Subjects:	SB Plant culture
Online Access:	https://ir.upsi.edu.my/detailsg.php?det=6429
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institution	Universiti Pendidikan Sultan Idris
collection	UPSI Digital Repository
language	eng
topic	SB Plant culture
spellingShingle	SB Plant culture Sharifah Norain Mohd Sharif Controlled release formulation of paddy pesticides intercalated layered metal hydroxide via polysaccharide encapsulation
description	This research aimed to synthesis intercalated nanocomposites of paddy pesticides forcontrolled release formulation (CRF), namely zinc/aluminiumlayered doublehydroxidequinclorac (Zn/AlLDHQC), zinc hydroxide nitratesodiumdodecylsulphatebispyribac (ZHNSDSBP) and zinc hydroxide nitratesodiumdodecylsulphateimidacloprid (ZHNSDSIC) using coprecipitation method. Surfacemodification of the nanocomposites, were then performed using carboxymethylcellulose (CMC) and chitosan coatings. The physicochemical properties, CRF andkinetic behaviour were monitored using powder Xray diffraction (PXRD),thermogravimetric analysis, Fourier transform infrared spectroscopy (FTIR), elementalanalysis, field emission scanning electron microscopy (FESEM), gas sorption analysisand ultravioletvisible spectrometer. The appearance of intercalation peaks at lower 2angle in the PXRD pattern, 15.816.7 ? (Zn/AlLDHQC), 28.228.6 ? (ZHNSDSBP) and 32.032.2 ? (ZHNSDSIC) confirmed the intercalation of pesticides in thenanocomposite, which also supported by FTIR and elemental analysis. All coatednanocomposites showed better performance in releasing pesticides, with prolongrelease time ranging from 24656083 min, compared to 14784117 min for theuncoated nanocomposites. Releasing of quinclorac and imidacloprid were governed bypseudo second order kinetic model, whereby the bispyribac was governed by pseudosecond order and parabolic diffusion kinetic models. In conclusion, the nanocompositesof paddy pesticides for CRF were successfully synthesised. The CMC and chitosancoatings obviously enhance the release behaviour of the pesticides from thenanocomposites. These synthesised nanocomposites are hopefully beneficial inovercoming the excessive usage of pesticide in paddy cultivation.
format	thesis
qualification_name
qualification_level	Doctorate
author	Sharifah Norain Mohd Sharif
author_facet	Sharifah Norain Mohd Sharif
author_sort	Sharifah Norain Mohd Sharif
title	Controlled release formulation of paddy pesticides intercalated layered metal hydroxide via polysaccharide encapsulation
title_short	Controlled release formulation of paddy pesticides intercalated layered metal hydroxide via polysaccharide encapsulation
title_full	Controlled release formulation of paddy pesticides intercalated layered metal hydroxide via polysaccharide encapsulation
title_fullStr	Controlled release formulation of paddy pesticides intercalated layered metal hydroxide via polysaccharide encapsulation
title_full_unstemmed	Controlled release formulation of paddy pesticides intercalated layered metal hydroxide via polysaccharide encapsulation
title_sort	controlled release formulation of paddy pesticides intercalated layered metal hydroxide via polysaccharide encapsulation
granting_institution	Universiti Pendidikan Sultan Idris
granting_department	Fakulti Sains dan Matematik
publishDate	2019
url	https://ir.upsi.edu.my/detailsg.php?det=6429
_version_	1747833263494266880
spelling	oai:ir.upsi.edu.my:64292021-11-12 Controlled release formulation of paddy pesticides intercalated layered metal hydroxide via polysaccharide encapsulation 2019 Sharifah Norain Mohd Sharif SB Plant culture This research aimed to synthesis intercalated nanocomposites of paddy pesticides forcontrolled release formulation (CRF), namely zinc/aluminiumlayered doublehydroxidequinclorac (Zn/AlLDHQC), zinc hydroxide nitratesodiumdodecylsulphatebispyribac (ZHNSDSBP) and zinc hydroxide nitratesodiumdodecylsulphateimidacloprid (ZHNSDSIC) using coprecipitation method. Surfacemodification of the nanocomposites, were then performed using carboxymethylcellulose (CMC) and chitosan coatings. The physicochemical properties, CRF andkinetic behaviour were monitored using powder Xray diffraction (PXRD),thermogravimetric analysis, Fourier transform infrared spectroscopy (FTIR), elementalanalysis, field emission scanning electron microscopy (FESEM), gas sorption analysisand ultravioletvisible spectrometer. The appearance of intercalation peaks at lower 2angle in the PXRD pattern, 15.816.7 ? (Zn/AlLDHQC), 28.228.6 ? (ZHNSDSBP) and 32.032.2 ? (ZHNSDSIC) confirmed the intercalation of pesticides in thenanocomposite, which also supported by FTIR and elemental analysis. All coatednanocomposites showed better performance in releasing pesticides, with prolongrelease time ranging from 24656083 min, compared to 14784117 min for theuncoated nanocomposites. Releasing of quinclorac and imidacloprid were governed bypseudo second order kinetic model, whereby the bispyribac was governed by pseudosecond order and parabolic diffusion kinetic models. In conclusion, the nanocompositesof paddy pesticides for CRF were successfully synthesised. The CMC and chitosancoatings obviously enhance the release behaviour of the pesticides from thenanocomposites. These synthesised nanocomposites are hopefully beneficial inovercoming the excessive usage of pesticide in paddy cultivation. 2019 thesis https://ir.upsi.edu.my/detailsg.php?det=6429 https://ir.upsi.edu.my/detailsg.php?det=6429 text eng closedAccess Doctoral Universiti Pendidikan Sultan Idris Fakulti Sains dan Matematik Abbad, S., Zhang, Z., Waddad, A. Y., Munyendo, W. L. L., Lv, H., & Zhou, J. (2015).Chitosan-modified cationic amino acid nanoparticles as a novel oral delivery system forinsulin. Journal of Biomedical Nanotechnology, 11(3), 486499.Abdul Latip, A. F., Hussein, M. Z., Stanslas, J., Wong, C. C., Adnan, R., Latip, A. F. A., Adnan,R. (2013). Release behavior and toxicity profiles towards A549 cell lines of ciprofloxacin fromits layered zinc hydroxide intercalation compound. 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