Simultaneously determination of bisphenol a and uric acid by zinc/aluminum-layered double hydroxide 2(2,4-dichlorophenoxy) propionate paste electrode

The purpose of this study was to determine simultaneously of bisphenol A and uric acid byzinc/aluminium-layered double hydroxide 2(2,4-dichlorophenoxy)propionate paste electrode. Themorphology of the electrode materials was performed by using scanning electron microscopy and transmission electro...

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Main Author:	Nurul Syahida Mat Aris
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Language:	eng
Published:	2020
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spellingShingle	Nurul Syahida Mat Aris Simultaneously determination of bisphenol a and uric acid by zinc/aluminum-layered double hydroxide 2(2,4-dichlorophenoxy) propionate paste electrode
description	The purpose of this study was to determine simultaneously of bisphenol A and uric acid byzinc/aluminium-layered double hydroxide 2(2,4-dichlorophenoxy)propionate paste electrode. Themorphology of the electrode materials was performed by using scanning electron microscopy and transmission electron microscopy. The electrochemical performance of modified pasteelectrode was studied by using cyclic voltammetry, square wave voltammetry, electrochemicalimpedance spectroscopy and chronocoulometry. Special importance effecting sensitivity andselectivity of the modified electrode must evaluated via optimization conditions which includeeffect of modifier composition percentage (15%), types of supporting electrolyte (PBS), pH ofelectrolyte (6.0) and square wave voltammetry parameters that encompassed of frequency(180Hz), pulse size (80mV) and step increment (7mV). The square wave voltammetry studies at anapplied potential of -0.30 V to + 1.0V, showed fast response within 1 second and detectedat high sensitivity. The modified sensor had showed a linear range from 5.0 M to 0.7 mM withdetection limit of 0.871 M and 0.795 M for bisphenol A and uric acid, respectively. Themodified sensors also exhibited good anti-interferences towards nitrate, chloride, sulphate, captopril, phthaldialdehyde, aspartic acid, glycine and fructose. In conclusion,the modified electrodes have been developed are able to detect bisphenol A and uricacid. By implication, the electrodes have been developed can be used as a suitable alternative forthe determination of bisphenol A and uric acid because it has characteristics suchas high sensitivity, reproducibility, repeatability and stability.
format	thesis
qualification_name
qualification_level	Master's degree
author	Nurul Syahida Mat Aris
author_facet	Nurul Syahida Mat Aris
author_sort	Nurul Syahida Mat Aris
title	Simultaneously determination of bisphenol a and uric acid by zinc/aluminum-layered double hydroxide 2(2,4-dichlorophenoxy) propionate paste electrode
title_short	Simultaneously determination of bisphenol a and uric acid by zinc/aluminum-layered double hydroxide 2(2,4-dichlorophenoxy) propionate paste electrode
title_full	Simultaneously determination of bisphenol a and uric acid by zinc/aluminum-layered double hydroxide 2(2,4-dichlorophenoxy) propionate paste electrode
title_fullStr	Simultaneously determination of bisphenol a and uric acid by zinc/aluminum-layered double hydroxide 2(2,4-dichlorophenoxy) propionate paste electrode
title_full_unstemmed	Simultaneously determination of bisphenol a and uric acid by zinc/aluminum-layered double hydroxide 2(2,4-dichlorophenoxy) propionate paste electrode
title_sort	simultaneously determination of bisphenol a and uric acid by zinc/aluminum-layered double hydroxide 2(2,4-dichlorophenoxy) propionate paste electrode
granting_institution	Universiti Pendidikan Sultan Idris
granting_department	Fakulti Sains dan Matematik
publishDate	2020
url	https://ir.upsi.edu.my/detailsg.php?det=6671
_version_	1747833288686305280
spelling	oai:ir.upsi.edu.my:66712022-02-08 Simultaneously determination of bisphenol a and uric acid by zinc/aluminum-layered double hydroxide 2(2,4-dichlorophenoxy) propionate paste electrode 2020 Nurul Syahida Mat Aris The purpose of this study was to determine simultaneously of bisphenol A and uric acid byzinc/aluminium-layered double hydroxide 2(2,4-dichlorophenoxy)propionate paste electrode. Themorphology of the electrode materials was performed by using scanning electron microscopy and transmission electron microscopy. The electrochemical performance of modified pasteelectrode was studied by using cyclic voltammetry, square wave voltammetry, electrochemicalimpedance spectroscopy and chronocoulometry. Special importance effecting sensitivity andselectivity of the modified electrode must evaluated via optimization conditions which includeeffect of modifier composition percentage (15%), types of supporting electrolyte (PBS), pH ofelectrolyte (6.0) and square wave voltammetry parameters that encompassed of frequency(180Hz), pulse size (80mV) and step increment (7mV). The square wave voltammetry studies at anapplied potential of -0.30 V to + 1.0V, showed fast response within 1 second and detectedat high sensitivity. The modified sensor had showed a linear range from 5.0 M to 0.7 mM withdetection limit of 0.871 M and 0.795 M for bisphenol A and uric acid, respectively. Themodified sensors also exhibited good anti-interferences towards nitrate, chloride, sulphate, captopril, phthaldialdehyde, aspartic acid, glycine and fructose. In conclusion,the modified electrodes have been developed are able to detect bisphenol A and uricacid. By implication, the electrodes have been developed can be used as a suitable alternative forthe determination of bisphenol A and uric acid because it has characteristics suchas high sensitivity, reproducibility, repeatability and stability. 2020 thesis https://ir.upsi.edu.my/detailsg.php?det=6671 https://ir.upsi.edu.my/detailsg.php?det=6671 text eng closedAccess Masters Universiti Pendidikan Sultan Idris Fakulti Sains dan Matematik A.Bulger, H., & E.Johns, H. (1941). The determination of Plasma Uric Acid.J.Biol.Chem, 140.Abdelwahab, A. A., & Shim, Y. B. (2015). Simultaneous determination of ascorbic acid, dopamine,uric acid and folic acid based on activated graphene/MWCNT nanocomposite loaded Aunanoclusters. Sensors and Actuators, B: Chemical, 221, 659665.Adams, R. N. (1958). Carbon Paste Electrodes. Analytical Chemistry, 30, 15761576.Ahmad, M. S., Isa, I., Hashim, N., Si, S. M., & Saidin, M. I. (2018). 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